in neat (no solvent) degassed ICl was treated with excess of Cl2 at ca. -50°C in the small greasless reactor, the reactor was warm up to room temp. for 30 min; excess of Cl2 was removed under vac. at -50;
参考文献
Journal of the American Chemical Society, , vol. 132, # 18 p. 6443 - 6462
in neat (no solvent) dropping IF5 to SOCl2 at room temp.;; condensation (cooling by liquid air); removal of ICl3 and Cl2 by Hg (shaking); fractionation;;
