4,4,5,5,6,6,7,7,7-九氟-1-庚烯-2-醇合成路线 （共 4 条）
反应条件
1: 88 percent / NH3 / diethyl ether / 1 h / Ambient temperature 2: 76 percent / aq. HCl / 1 h / Heating View Scheme
参考文献
Kurykin; Vol'pin; German
Journal of Fluorine Chemistry, 1996 , vol. 80, # 1 p. 9 - 12
反应条件
potassium hydroxide in acetone
electrolysis;
参考文献
Vol'pin, I. M.; Kurykin, M. A.; Grinberg, V. A.; Vasil'ev, Yu. B.; German, L. S.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1991 , vol. 40, # 7 p. 1395 - 1400
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1991 , # 7 p. 1578 - 1584
反应条件
2,2'-azo-bisisobutyronitrile; acide sulfurique; N-ethyl-N,N-diisopropylamine
1.) pentane, 100 deg C, heating in autoclave, 6 h; 2.) water, 16 h;
参考文献
Molines, Huguette; Tordeux, Marc; Wakselman, Claude
Bulletin de la Societe Chimique de France, 1982 , vol. 2, # 11-12 p. 367 - 368
反应条件
electrolysis, platinum or glasscarbon electrodes; Yield given;
参考文献
Vol'pin, I. M.; Kurykin, M. A.; Grinberg, V. A.; German, L. S.
Journal of Fluorine Chemistry, 1991 , vol. 54, # 1-3 p. 303
