反应条件
1: 73 percent / NaBH4, BF3*O(C2H5)2 / tetrahydrofuran
2: 98 percent / HBr / H2O; H2SO4 / Heating
3: 84 percent / Na2S*9H2O / H2O; methanol / Heating
4: 89 percent / 30 percent H2O2 / acetic acid; H2O / 1.5 h / Heating
5: 1) n-butyllithium / 1) benzene, ether, hexane, tetrahydrofuran,
6: 1) SOCl2 / 1) benzene, 3 h, reflux, 2) 2 h
View Scheme
参考文献
Sindelar, Karel; Holubek, Jiri; Ryska, Miroslav; Koruna, Ivan; Protiva, Miroslav
Collection of Czechoslovak Chemical Communications, 1986 , vol. 51, # 12 p. 2848 - 2868
