Alpha-氰基-3,4-二甲氧基肉桂酸合成路线 （共 10 条）
反应条件
sodium hydroxide; sodium hypochlorite; carbon dioxide
参考文献
McRae; Hopkins
Canadian Journal of Research, 1932 , vol. 7, p. 248,255
反应条件
1: 80 percent / NaBH4 / methanol 2: 91 percent / dimethylformamide / Heating 3: 60 percent / LiAlH4 / tetrahydrofuran View Scheme
参考文献
Vincze, Zoltan; Biro, A. Beatrix; Csekei, Marton; Timari, Geza; Kotschy, Andras
Synthesis, 2006 , # 8 p. 1375 - 1385
反应条件
ammonium acetate in toluene
Knoevenagel condensation;
参考文献
Vincze, Zoltan; Biro, A. Beatrix; Csekei, Marton; Timari, Geza; Kotschy, Andras
Synthesis, 2006 , # 8 p. 1375 - 1385
反应条件
piperidine in benzene
Ambient temperature;
参考文献
Manrao, M. R.; Kaur, Baljit; Sharma, R. C.; Kalsi, P. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 11 p. 1059 - 1060
反应条件
sodium hydroxide
T=50°C;
参考文献
Baker; Robinson
Journal of the Chemical Society, 1925 , vol. 127, p. 1433
反应条件
hydrogenchloride; acetic acid
参考文献
van Duin
Recueil des Travaux Chimiques des Pays-Bas, 1926 , vol. 45, p. 358
Recueil des Travaux Chimiques des Pays-Bas, 1928 , vol. 47, p. 734
参考文献
Richardson et al.
Journal of the Chemical Society, 1937 , p. 835,839
Full Text Show Details
Dave; Trivedi; Nargund
Journal of the University of Bombay, Science: Physical Sciences, Mathematics, Biological Sciences and Medicine, 1943 , vol. 11/5 A, p. 111
反应条件
1: diluted KOH-solution / Darst.
2: piperidine / 100 °C
3: glacial acetic acid; concentrated hydrochloric acid
View Scheme
参考文献
van Duin
Recueil des Travaux Chimiques des Pays-Bas, 1926 , vol. 45, p. 358
Recueil des Travaux Chimiques des Pays-Bas, 1928 , vol. 47, p. 734
反应条件
1: 80 percent / NaBH4 / methanol
2: 91 percent / dimethylformamide / Heating
View Scheme
参考文献
Baker; Robinson
Journal of the Chemical Society, 1925 , vol. 127, p. 1433
反应条件
sodium tetrahydroborate in methanol
参考文献
Vincze, Zoltan; Biro, A. Beatrix; Csekei, Marton; Timari, Geza; Kotschy, Andras
Synthesis, 2006 , # 8 p. 1375 - 1385
