4,4'-二(三氟甲基)-2,2'-二硝基二苯基二硫醚合成路线 （共 13 条）
反应条件
dipotassium N-cyano-dithioimidocarbonate in N,N-dimethyl-formamide T=80 - 90°C; 24 h;
参考文献
Ruminski, Peter G.; Suba, Lydia A.; D'Amico, John J.
Phosphorus and Sulfur and the Related Elements, 1984 , vol. 19, p. 335 - 344
反应条件
sodium sulfide in carbon disulfide; butanone 12 h; Ambient temperature;
参考文献
Gazzetta Chimica Italiana, , vol. 110, # 5/6 p. 301 - 304
反应条件
sodium sulfide in ethanol; water 1 h; Heating;
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 46, # 1 p. 118 - 140
参考文献
Hogg,D.R.; Stewart,J.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1974 , p. 436 - 441
反应条件
hydrogenchloride; acetic acid; zinc anschliessendes Erhitzen mit Acetanhydrid;
参考文献
Kiprianow; Jagupol'skii
Zhurnal Obshchei Khimii, 1952 , vol. 22, p. 2209,2214; engl. Ausg. S. 2267, 2271
反应条件
hydrogenchloride; tin
参考文献
Gupta, R. R.; Kumar, Rakesh
Journal of Fluorine Chemistry, 1986 , vol. 31, p. 19 - 24
反应条件
1.1: alpha-D-glucopyranose / ethanol / 0.17 h / 55 °C 1.2: 0.17 h / 20 °C 2.1: potassium hydroxide / ethanol / 0.17 h / 20 °C 2.2: 0.33 h / 40 - 45 °C View Scheme
参考文献
Rodygin, Konstantin S.; Rubtsova, Svetlana A.; Kutchin, Alexander V.; Slepukhin, Pavel A.
Phosphorus, Sulfur and Silicon and the Related Elements, 2011 , vol. 186, # 9 p. 1885 - 1894
反应条件
1: zinc; aqueous HCl; acetic acid / anschliessendes Erhitzen mit Acetanhydrid 2: aqueous H2SO4 View Scheme
参考文献
Kiprianow; Jagupol'skii
Zhurnal Obshchei Khimii, 1952 , vol. 22, p. 2209,2214; engl. Ausg. S. 2267, 2271
反应条件
1.1: alpha-D-glucopyranose / ethanol / 0.17 h / 55 °C 1.2: 0.17 h / 20 °C 2.1: potassium hydroxide / ethanol / 0.17 h / 20 °C 2.2: 0.33 h / 40 - 45 °C View Scheme
参考文献
Rodygin, Konstantin S.; Rubtsova, Svetlana A.; Kutchin, Alexander V.; Slepukhin, Pavel A.
Phosphorus, Sulfur and Silicon and the Related Elements, 2011 , vol. 186, # 9 p. 1885 - 1894
反应条件
1: With alpha-D-glucopyranose in ethanol T=55°C; 0.166667 h; 2: With potassium hydroxide in ethanol T=20°C; 0.166667 h;
参考文献
Rodygin, Konstantin S.; Rubtsova, Svetlana A.; Kutchin, Alexander V.; Slepukhin, Pavel A.
Phosphorus, Sulfur and Silicon and the Related Elements, 2011 , vol. 186, # 9 p. 1885 - 1894
