3,4,5-三甲氧基苯甲醛合成路线 （共 427 条）
反应条件
sodium periodate; osmium(VIII) oxide; N-benzyl-N,N,N-triethylammonium chloride in tetrahydrofuran; water 0.0166667 h; microwave irradiation;
参考文献
Sinha, Arun K.; Joshi, Bhupendra P.; Acharya, Ruchi
Chemistry Letters, 2003 , vol. 32, # 8 p. 780 - 781
反应条件
aluminum oxide; potassium permanganate T=20°C; 0.0166667 h;
参考文献
Imanzadeh Karkaragh; Eskandari
Indian Journal of Chemistry - Section A Inorganic, Physical, Theoretical and Analytical Chemistry, 2005 , vol. 44, # 7 p. 1392 - 1394
反应条件
1: 95 percent / Br2 / acetic acid / 1 h 2: 83 percent / CuCl2 / dimethylformamide; methanol / 1 h / 100 °C 3: 96 percent / NaOH / Adogen 464 / H2O; CH2Cl2 / 16 h / Ambient temperature View Scheme
参考文献
Synthesis, , # 4 p. 308
反应条件
NiCl2((PPh3)P)2; tetra-(n-butyl)ammonium iodide; (S)-(+)-(3,5-dioxa-4-phosphacyclohepta[2,1-a:3,4-a']dinaphthalen-4-yl)diethylamine; zinc in N,N-dimethyl acetamide T=45°C; Ullmann reaction; 4 h; Inert atmosphere; optical yield given as percent eeenantioselective reaction;
参考文献
Organic Letters, , vol. 12, # 5 p. 1072 - 1075
反应条件
dichloro bis(acetonitrile) palladium(II); water; oxygen; copper dichloride in toluene; tert-butyl alcohol T=60°C; Wacker Oxidation; P=6000.6 Torr; 1 h; Flow reactor;
参考文献
Advanced Synthesis and Catalysis, , vol. 355, # 10 p. 1905 - 1910
反应条件
sodium carbonate in acetone 5 h; Heating;
参考文献
Synthetic Communications, , vol. 28, # 9 p. 1517 - 1524
反应条件
silica gel Hydrolysis;
参考文献
Paredes, Maria Dolores; Alonso, Ricardo
Tetrahedron Letters, 1999 , vol. 40, # 20 p. 3973 - 3976
反应条件
1: tetrabutylammomium bromide; potassium hydroxide / 0.67 h / 100 °C / Neat (no solvent) 2: pyridine; ozone / methanol; chloroform / -15 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 21, # 6 p. 1578 - 1581
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in dichloromethane; water T=20°C; 1 h;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 36, # 10 p. 4244 - 4247
