3,4,5-三甲氧基苯甲醛合成路线 （共 427 条）
反应条件
sodium hydride
1.) DMSO, 90 deg C, 0.5 h; 2.) r.t., 1 h; Yield given. Multistep reaction;
参考文献
Center for Innovative Technology
Patent: US5530141 A1, 1996 ;
反应条件
caesium carbonate in tetrahydrofuran
T=80°C; 12 h;
参考文献
Forbes, David C.; Bettigeri, Sampada V.; Patrawala, Samit A.; Pischek, Susanna C.; Standen, Michael C.
Tetrahedron, 2009 , vol. 65, # 1 p. 70 - 76
反应条件
sodium hydroxide; tetrabutylammomium bromide in dichloromethane
T=50°C; 96 h;
参考文献
Alvarez; Granados; Lavilla; Salas
Journal of Heterocyclic Chemistry, 1985 , vol. 22, # 3 p. 745 - 750
反应条件
sodium hydroxide in dichloromethane; water
T=50°C; Corey-Chaykovsky reaction; Phase-transfer catalyst;
参考文献
Afon'kin; Kostrikin; Shumeiko; Popov
Russian Journal of Organic Chemistry, 2008 , vol. 44, # 12 p. 1776 - 1779
反应条件
in dimethyl sulfoxide
参考文献
KYOWA HAKKO KOGYO CO., LTD.
Patent: EP812825 A1, 1997 ;
参考文献
Somei, Masanori; Aoki, Kazuko; Nagahama, Yoshiyuki; Nakagawa, Kyoko
Heterocycles, 1995 , vol. 41, # 1 p. 5 - 8
反应条件
in tetrahydrofuran; dimethyl sulfoxide
1.) 0-5 deg C, 15 min., 2.) r.t., 90 min; Yield given;
参考文献
Alvarez; Granados; Lavilla; Salas
Journal of Heterocyclic Chemistry, 1985 , vol. 22, # 3 p. 745 - 750
反应条件
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride
1a) 0 deg C, 15 min, 1b) benzene, 18-20 deg C, few minutes, 2) benzene, 50 deg C, 10 h; Yield given. Multistep reaction;
参考文献
Haridas, K.; Dev, Sukh
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1987 , vol. 26, # 1-12 p. 1018 - 1020
反应条件
sodium peroxodisulphate; sulfuric acid; nitric acid
T=-8°C;
参考文献
Sharp
Journal of the Chemical Society, 1936 , p. 1234
参考文献
Sharp
Journal of the Chemical Society, 1936 , p. 1234
