3,4,5-三甲氧基苯甲醛合成路线 （共 427 条）
反应条件
polymethylhydrosiloxane; trifuran-2-yl-phosphane; tetrabutyl ammonium fluoride; potassium fluoride; tris-(dibenzylideneacetone)dipalladium(0) in tetrahydrofuran; water T=20°C; 1 h;
参考文献
Lee, Kyoungsoo; Maleczka Jr., Robert E.
Organic Letters, 2006 , vol. 8, # 9 p. 1887 - 1888
反应条件
tert.-butylhydroperoxide; V/SiO2 in decane; tert-butyl alcohol T=25°C; 5 h;
参考文献
Rout, Laxmidhar; Nath, Pinku; Punniyamurthy, Tharmalingam
Advanced Synthesis and Catalysis, 2007 , vol. 349, # 6 p. 846 - 848
反应条件
bis(acetylacetonato) palladium; hydrogen; trimethylacetic anhydride; phenyldicyclohexylphosphine in tetrahydrofuran T=80°C; P=3750.38 Torr; 20 h; Inert atmosphere;
参考文献
Goossen, Lukas J.; Khan, Bilal Ahmad; Fett, Thomas; Treu, Matthias
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 13 p. 2166 - 2170
反应条件
ammonium hydroxide; potassium hexacyanoferrate(III) in dichloromethane; water T=20°C; 4 h;
参考文献
Chida; Vani; Chandrasekharam; Srinivasan; Singh
Synthetic Communications, 2001 , vol. 31, # 5 p. 657 - 660
反应条件
antimony(V) pentachloride in dichloromethane T=20°C; 2 h;
参考文献
Hangarge; Mane; Chavan; Shingare
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2002 , vol. 41, # 6 p. 1302 - 1304
反应条件
1: With acetyl chloride; sodium nitrite in dichloromethane T=0 - 5°C; 0.25 h; 2: With water in dichloromethane T=0 - 20°C; 1.25 h;
参考文献
Khan, Abu T.; Mondal, Ejabul; Sahu, Priti R.
Synlett, 2003 , # 3 p. 377 - 381
反应条件
sodium hydroxide; adogen 464 in dichloromethane; water 16 h; Ambient temperature;
参考文献
Rao, Durvasula V.; Stuber, F. A.
Synthesis, 1983 , # 4 p. 308
反应条件
trifluoroacetic acid in dichloromethane T=25°C; 16 h;
参考文献
Li, Wei; Li, Jianchang; Wu, Yuchuan; Fuller, Nathan; Markus, Michelle A.
Journal of Organic Chemistry, 2010 , vol. 75, # 4 p. 1077 - 1086
反应条件
triethylene diamine nickel thiosulfate; water in chloroform T=20°C; Hydrolysis; 0.0833333 h;
参考文献
Kamal; Arifuddin; Rao
Synlett, 2000 , # 10 p. 1482 - 1484
反应条件
1: With tert.-butylnitrite in benzene Nitrosation; 2: in benzene T=0°C; Elimination; Photolysis; Further stages.;
参考文献
Paredes; Alonso
Journal of Organic Chemistry, 2000 , vol. 65, # 8 p. 2292 - 2304
