N,N-二甲基-1-萘胺合成路线 （共 67 条）
反应条件
und anschliessend mit H2O;
参考文献
Benkeser et al.
Journal of the American Chemical Society, 1958 , vol. 80, p. 6573,6576
Journal of Organic Chemistry, 1959 , vol. 24, p. 854
反应条件
1: dichloromethane / 4 h / 20 °C / |Inert atmosphere; |Schlenk technique
2: iron (III) acetylacetonate / tetrahydrofuran; 1-methyl-pyrrolidin-2-one / 1 h / 25 °C / |Inert atmosphere; |Schlenk technique
View Scheme
参考文献
Guo, Wang-Jun; Wang, Zhong-Xia
Tetrahedron, 2013 , vol. 69, # 46 p. 9580 - 9585
反应条件
1: dichloromethane / 4 h / 20 °C / |Inert atmosphere; |Schlenk technique
2: iron (III) acetylacetonate / tetrahydrofuran; 1-methyl-pyrrolidin-2-one / 1 h / 25 °C / |Inert atmosphere; |Schlenk technique
View Scheme
参考文献
Guo, Wang-Jun; Wang, Zhong-Xia
Tetrahedron, 2013 , vol. 69, # 46 p. 9580 - 9585
反应条件
n-butyllithium
1.) ether, room temp., 48 h; 2.) ether, -78 deg C up to -20 deg C within 4 h; Yield given. Multistep reaction;
参考文献
Kirby, Anthony J.; Percy, Jonathan M.
Tetrahedron, 1988 , vol. 44, # 22 p. 6903 - 6910
参考文献
Friedlaender; Welmans
Chemische Berichte, 1888 , vol. 21, p. 3125
Show Details
Scharwin; Kaljanow
Chemische Berichte, 1908 , vol. 41, p. 2058
反应条件
n-butyllithium; N,N,N',N,-tetramethylethylenediamine
1.) n-hexane, 2.) n-hexane; Yield given. Multistep reaction;
参考文献
Horner, L.; Simons, G.
Phosphorus and Sulfur and the Related Elements, 1983 , vol. 15, p. 165 - 176
参考文献
State of Oregon
Patent: US5262568 A1, 1993 ;
US 5262568 A
参考文献
v.Braun; Heider; Mueller
Chemische Berichte, 1918 , vol. 51, p. 279
参考文献
v.Braun; Heider; Mueller
Chemische Berichte, 1918 , vol. 51, p. 279
反应条件
pyridine; tert.-butylhydroperoxide; iron(II) chloride in acetonitrile
T=85°C; 2 h; Inert atmosphere; chemoselective reaction;
参考文献
Li, Yuanming; Ma, Lina; Jia, Fan; Li, Zhiping
Journal of Organic Chemistry, 2013 , vol. 78, # 11 p. 5638 - 5646
