N,N-二甲基-1-萘胺合成路线 （共 67 条）
反应条件
N-fluoro-N-(phenylsulfonyl)benzene-sulfonamide in chloroform T=25°C; 10 h;
参考文献
Journal of Fluorine Chemistry, , vol. 154, p. 67 - 72
反应条件
N-fluoro-N-(phenylsulfonyl)benzene-sulfonamide in chloroform T=25°C; 10 h;
参考文献
Journal of Fluorine Chemistry, , vol. 154, p. 67 - 72
反应条件
1: dichloromethane / 4 h / 20 °C / |Inert atmosphere; |Schlenk technique 2: iron (III) acetylacetonate / tetrahydrofuran; 1-methyl-pyrrolidin-2-one / 1 h / 25 °C / |Inert atmosphere; |Schlenk technique View Scheme
参考文献
Guo, Wang-Jun; Wang, Zhong-Xia
Tetrahedron, 2013 , vol. 69, # 46 p. 9580 - 9585
参考文献
Paras, Nick A.; Simmons, Bryon; MacMillan, David W.C.
Tetrahedron, 2009 , vol. 65, # 16 p. 3232 - 3238
反应条件
1,4-diaza-bicyclo[2.2.2]octane in chloroform Friedel-Crafts acylation; 22 h; Heating;
参考文献
Synthesis, , # 6 p. 904 - 908
反应条件
T=60 - 70°C; Uebersaettigen des Reaktionsproduktes mit NaOH und Zerstzung der alkalischer loesung mit Essigsaeure;
参考文献
Friedlaenger; Welmans
Chemische Berichte, 1888 , vol. 21, p. 3126
反应条件
pyridine in acetonitrile 1 h; Ambient temperature;
参考文献
Synthesis, , # 1 p. 22 - 25
反应条件
1: 4-nitro-aniline With hydrogenchloride; sodium nitrite in water T=0 - 4°C; 0.25 h; 2: 1-N,N-dimethylaminonaphthalene With potassium acetate in water; acetic acid T=20°C; 1.5 h; Cooling with ice;
参考文献
Rolic AG
Patent: EP1256602 A1, 2002 ;
Location in patent: Page 14 ;
参考文献
Huenig; Requardt
Justus Liebigs Annalen der Chemie, 1955 , vol. 592, p. 180,188
反应条件
N-fluoro-N-(phenylsulfonyl)benzene-sulfonamide in chloroform T=25°C; 10 h;
参考文献
Journal of Fluorine Chemistry, , vol. 154, p. 67 - 72
