2,3-二甲氧基苯甲醛合成路线 （共 174 条）
参考文献
Chemische Berichte, , vol. 46, p. 4024
参考文献
Chemische Berichte, , vol. 51, p. 123
反应条件
1: sodium tetrahydroborate / methanol / 0.17 h / 20 °C 2: N-bromosuccinmide / tetrahydrofuran / 20 °C View Scheme
参考文献
De, Subhadip; Chaudhuri, Saikat; Mishra, Sourabh; Mamtani, Himanshu; Bisai, Alakesh
Journal of the Indian Chemical Society, 2013 , vol. 90, # 10 p. 1871 - 1884
反应条件
1.1: 85 percent / 1 h / 110 °C 2.1: 85 percent / NaBH4 / methanol / 2 h / Heating 3.1: HOAc; CuSO4; NaCl / 0.5 h / 50 °C 3.2: 60 percent / AcOH / 6 h / 85 °C View Scheme
参考文献
Bian, Xiaoli; He, Langchong; Yang, Guangde
Bioorganic and Medicinal Chemistry Letters, 2006 , vol. 16, # 5 p. 1380 - 1383
反应条件
1: permanganate 2: hydrogen iodide / 100 °C 3: aqueous-alcoholic KOH-solution; hydrogen stream View Scheme
参考文献
Perkin; Trikojus
Journal of the Chemical Society, 1926 , p. 2932
反应条件
ammonium acetate; acetic acid T=22°C; 3 h; ultrasound;
参考文献
McNulty, James; Steere, Jennifer A.; Wolf, Sonja
Tetrahedron Letters, 1998 , vol. 39, # 44 p. 8013 - 8016
参考文献
Gairaud; Lappin
Journal of Organic Chemistry, 1953 , vol. 18, p. 1
反应条件
PhNHCO2NH2*TsOH in toluene Condensation; elimination; 0.5 h; Heating;
参考文献
Coskun, Necdet; Arikan, Nevin
Tetrahedron, 1999 , vol. 55, # 40 p. 11943 - 11948
反应条件
1: CH2Cl2 / 24 h / 20 °C 2: LiAlH4 / tetrahydrofuran / 2 h / 20 °C 3: Et3N / CH2Cl2 / 0.33 h / 0 °C 4: SnCl4 / CH2Cl2 / 1 h / 0 °C 5: 77 percent / Raney Ni / ethanol / 2 h / Heating 6: POCl3; K2CO3 / acetonitrile / 0.67 h / 60 °C View Scheme
参考文献
Hanaoka, Miyoji; Hirasawa, Taeko; Cho, Won Jea; Yasuda, Shingo
Chemical and Pharmaceutical Bulletin, 2000 , vol. 48, # 3 p. 399 - 404
反应条件
sodium tetrahydroborate in methanol T=20°C; 0.166667 h;
参考文献
De, Subhadip; Chaudhuri, Saikat; Mishra, Sourabh; Mamtani, Himanshu; Bisai, Alakesh
Journal of the Indian Chemical Society, 2013 , vol. 90, # 10 p. 1871 - 1884
