2,2-二甲基-4(s)-4-叠氮基甲基-1,3-二氧杂烷合成路线 （共 7 条）
反应条件
hydrogenchloride; hydrogen; palladium on activated charcoal in methanol
参考文献
Lepine, Renaud; Carbonnelle, Anny-Claude; Zhu, Jieping
Synlett, 2003 , # 10 p. 1455 - 1458
反应条件
sodium azide in dimethyl sulfoxide
T=100°C;
参考文献
Lepine, Renaud; Carbonnelle, Anny-Claude; Zhu, Jieping
Synlett, 2003 , # 10 p. 1455 - 1458
反应条件
1: 70 percent / pyridine
2: 40 percent / NaN3 / dimethylformamide / 12 h / 60 °C
View Scheme
参考文献
Barili; Biagi; Giorgi; Livi; Scartoni
Journal of Heterocyclic Chemistry, 1991 , vol. 28, # 5 p. 1351 - 1355
反应条件
1: 45 percent
2: 70 percent / pyridine
3: 40 percent / NaN3 / dimethylformamide / 12 h / 60 °C
View Scheme
参考文献
Barili; Biagi; Giorgi; Livi; Scartoni
Journal of Heterocyclic Chemistry, 1991 , vol. 28, # 5 p. 1351 - 1355
反应条件
1: sodium tetrahydroborate / ethanol / 0 °C
2: triethylamine / 2 h / 0 °C
3: sodium azide / N,N-dimethyl-formamide / 90 °C
View Scheme
参考文献
Ganesan; Muraleedharan
Nucleosides, Nucleotides and Nucleic Acids, 2010 , vol. 29, # 2 p. 91 - 96
反应条件
1: sodium periodate; sodium hydrogencarbonate / dichloromethane / 1 h
2: sodium tetrahydroborate / ethanol / 0 °C
3: triethylamine / 2 h / 0 °C
4: sodium azide / N,N-dimethyl-formamide / 90 °C
View Scheme
参考文献
Ganesan; Muraleedharan
Nucleosides, Nucleotides and Nucleic Acids, 2010 , vol. 29, # 2 p. 91 - 96
反应条件
hydrogen; palladium on activated charcoal in methanol
5 h; Ambient temperature;
参考文献
Schmidt, Ulrich; Meyer, Regina; Leitenberger, Volker; Lieberknecht, Albrecht; Griesser, Helmut
Journal of the Chemical Society, Chemical Communications, 1991 , # 5 p. 275 - 277
