反应条件
1: 95 percent / imidazole / dimethylformamide / 3 h / 20 °C
2: 98 percent / K2CO3 / methanol / 2 h
3: PCC / CH2Cl2 / 1 h / 20 °C
4: K2CO3 / methanol / 1.5 h / 20 °C
5: 550 mg / LiAlH4 / diethyl ether / 3 h / 0 °C
6: CBr4; PPh3 / benzene / 2 h / 0 °C
7: 75 percent / Mn / Cp2TiCl2 / tetrahydrofuran / 20 °C
8: 90 percent / TBAF / tetrahydrofuran / 11 h / 60 °C
View Scheme
参考文献
Barrero, Alejandro F.; Herrador, M. Mar; Del Moral, Jose F. Quilez; Arteaga, Pilar; Arteaga, Jesus F.; Piedra, Maria; Sanchez, Elena M.
Organic Letters, 2005 , vol. 7, # 12 p. 2301 - 2304
