2-(二甲基氨基)-4-甲基噻唑-5-甲醛合成路线 (共 2 条)
反应条件
trichlorophosphate
T=40°C; 4 h;
参考文献
Gillon, David W.; Forrest, Ian J.; Meakins, G. Denis; Tirel, Malcolm D.; Wallis, John D.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 341 - 348
反应条件
n-butyllithium
1) -78 deg C, 10 min., hexane, THF, 2) up to room temp., 2h; Yield given. Multistep reaction;
参考文献
Sawhney, Indu; Wilson, John R. H.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 2 p. 329 - 331