titanium tetrachloride in 1,2-dichloro-benzene
T=115 - 125°C; 0.5 h;
参考文献
Ito, Suketaka; Tanaka, Yumo; Kakehi, Akikazu; Fukuyama, Toshihiko; Osawa, Nobuo; Sayo, Noboru
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 2 p. 545 - 548
1: 18 percent / dioxane / 24 h / Heating; without solvent, other temp. (105-110 deg C)
2: 78 percent / NaH / dioxane / 20 h / Heating; under nitrogen
View Scheme
参考文献
Ito, Suketaka; Tanaka, Yumo; Kakehi, Akikazu
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 2 p. 544 - 547
titanium tetrachloride in 1,2-dichloro-benzene
T=115 - 125°C; 0.5 h;
参考文献
Ito, Suketaka; Tanaka, Yumo; Kakehi, Akikazu; Fukuyama, Toshihiko; Osawa, Nobuo; Sayo, Noboru
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 2 p. 545 - 548
1: 13.0 g / ammonia / dimethylformamide / 0.5 h / 80 °C
2: 77 percent / 3.5 h / 145 - 155 °C
View Scheme
参考文献
Ito, Suketaka; Tanaka, Yumo; Kakehi, Akikazu; Fukuyama, Toshihiko; Osawa, Nobuo; Sayo, Noboru
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 2 p. 545 - 548
