辛基 2,3,4,6-四-O-乙酰基-beta-D-硫代吡喃葡萄糖苷合成路线 （共 7 条）
反应条件
2,2'-azo-bisisobutyronitrile in acetonitrile T=80°C; 0.25 h;
参考文献
Lacombe, J. M.; Rakotomanomana, N.; Pavia, A. A.
Tetrahedron Letters, 1988 , vol. 29, # 34 p. 4293 - 4296
反应条件
potassium carbonate; sodium hydrogensulfite in water; acetone Ambient temperature;
参考文献
Saito, Setsuo; Tsuchiya, Tomofusa
Chemical & Pharmaceutical Bulletin, 1985 , vol. 33, # 2 p. 503 - 508
反应条件
1: 95 percent / acetone / 0.5 h / Heating 2: 96 percent / K2CO3, NaHSO3 / acetone; H2O / Ambient temperature View Scheme
参考文献
Chemical & Pharmaceutical Bulletin, , vol. 33, # 2 p. 503 - 508
反应条件
1: 91.7 percent / red phosphorus, bromine, aq. HBr / acetic anhydride / 1 h / 40 - 50 °C 2: 95 percent / acetone / 0.5 h / Heating 3: 96 percent / K2CO3, NaHSO3 / acetone; H2O / Ambient temperature View Scheme
参考文献
Chemical & Pharmaceutical Bulletin, , vol. 33, # 2 p. 503 - 508
反应条件
boron trifluoride diethyl etherate in diethyl ether; chloroform 8 h; Ambient temperature; Yield given;
参考文献
Carbohydrate Research, , vol. 194, p. 71 - 78
反应条件
boron trifluoride diethyl etherate in chloroform 0.25 h;
参考文献
Molecular Crystals and Liquid Crystals Science and Technology Section A: Molecular Crystals and Liquid Crystals, , vol. 260, # pt 1 p. 185 - 199
反应条件
sodium hydroxide in methanol Ambient temperature;
参考文献
Galema, Saskia A.; Engberts, Jan B. F. N.; Van Doren, Henk A.
Carbohydrate Research, 1997 , vol. 303, # 4 p. 423 - 434
