7,8-二氢-6H-5-氧杂-9-硫杂-苯并环庚烯-7-醇合成路线 （共 5 条）
反应条件
sodium tetrahydroborate in ethanol
2 h; Ambient temperature;
参考文献
Sugihara; Mabuchi; Kawamatsu
Chemical and pharmaceutical bulletin, 1987 , vol. 35, # 5 p. 1919 - 1929
反应条件
sodium hydroxide
15 h; Heating;
参考文献
Cabiddu, Salvatore; Melis, Stefana; Sotgiu, Francesca; Cerioni, Giovanni
Phosphorus and Sulfur and the Related Elements, 1982 , vol. 14, p. 151 - 156
反应条件
1: 83 percent / K2CO3 / 5 h / Heating
2: 71 percent / 28percent NaOCH3 / dimethylformamide / 1 h / Ambient temperature
3: 79 percent / 65percent H2SO4 / acetic acid / 1 h / Heating
4: 60 percent / sodium borohydride / ethanol / 2 h / Ambient temperature
View Scheme
参考文献
Sugihara; Mabuchi; Kawamatsu
Chemical and pharmaceutical bulletin, 1987 , vol. 35, # 5 p. 1919 - 1929
反应条件
1: 71 percent / 28percent NaOCH3 / dimethylformamide / 1 h / Ambient temperature
2: 79 percent / 65percent H2SO4 / acetic acid / 1 h / Heating
3: 60 percent / sodium borohydride / ethanol / 2 h / Ambient temperature
View Scheme
参考文献
Sugihara; Mabuchi; Kawamatsu
Chemical and pharmaceutical bulletin, 1987 , vol. 35, # 5 p. 1919 - 1929
反应条件
1: 79 percent / 65percent H2SO4 / acetic acid / 1 h / Heating
2: 60 percent / sodium borohydride / ethanol / 2 h / Ambient temperature
View Scheme
参考文献
Sugihara; Mabuchi; Kawamatsu
Chemical and pharmaceutical bulletin, 1987 , vol. 35, # 5 p. 1919 - 1929
