2,3-二溴-2-甲基丁腈合成路线 (共 3 条)
反应条件
methanecarbohydroxamic acid; sodium methylate in methanol T=64°C; 18 h; Inert atmosphere;
参考文献
Tellew, John E.; Leith, Leslie; Mathur, Arvind
Organic Process Research and Development, 2007 , vol. 11, # 2 p. 275 - 277
反应条件
1: With 1,8-diazabicyclo[5.4.0]undec-7-ene in dichloromethane
T=0 - 20°C; 16 h; Inert atmosphere;
2: With bromine in dichloromethane
T=0 - 20°C; 17.5 h;
参考文献
Tellew, John E.; Leith, Leslie; Mathur, Arvind
Organic Process Research and Development, 2007 , vol. 11, # 2 p. 275 - 277
反应条件
bromine in tetrachloromethane
Heating;
参考文献
Chalchat,J.C.; Theron,F.
Bulletin de la Societe Chimique de France, 1974 , p. 953 - 957