(R)-1,2-十二烷二醇合成路线 （共 9 条）
反应条件
1: H2; NEt3 / 10percent Pd/C / methanol / 24 h / 20 °C 2: aq. HCl / methanol / 20 °C View Scheme
参考文献
Chemistry - A European Journal, , vol. 9, # 1 p. 282 - 290
反应条件
1: 90 percent 2: 95 percent / H2 / Pd-C / ethanol 3: HCl / methanol View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 39, # 11 p. 1934 - 1937
反应条件
hydrogenchloride in methanol Ring cleavage;
参考文献
Angewandte Chemie - International Edition, , vol. 39, # 11 p. 1934 - 1937
反应条件
1.1: 2.5 h / 140 °C 2.1: BuLi / tetrahydrofuran / 0.5 h / -20 °C 2.2: tetrahydrofuran / 4 h / 20 °C 3.1: H2; NEt3 / 10percent Pd/C / methanol / 24 h / 20 °C 4.1: aq. HCl / methanol / 20 °C View Scheme
参考文献
Chemistry - A European Journal, , vol. 9, # 1 p. 282 - 290
反应条件
1.1: BuLi / tetrahydrofuran / 0.5 h / -20 °C 1.2: tetrahydrofuran / 4 h / 20 °C 2.1: H2; NEt3 / 10percent Pd/C / methanol / 24 h / 20 °C 3.1: aq. HCl / methanol / 20 °C View Scheme
参考文献
Chemistry - A European Journal, , vol. 9, # 1 p. 282 - 290
反应条件
K2OsO2(OH)4; hydroquinidine 1,4-phthalazinediyl diether; iodine; potassium carbonate in water; tert-butyl alcohol Overall yield = 97 percent;
参考文献
European Journal of Organic Chemistry, , # 30 p. 6886 - 6899
反应条件
1: NaBH4 / methanol 2: catalytic hydrogenolysis View Scheme
参考文献
Journal of the Chemical Society - Series Chemical Communications, , vol. No. 22, p. 1285 - 1286
反应条件
1: 80 percent / HIO4 / tetrahydrofuran / Ambient temperature 2: NaBH4 / methanol 3: catalytic hydrogenolysis View Scheme
参考文献
Journal of the Chemical Society - Series Chemical Communications, , vol. No. 22, p. 1285 - 1286
反应条件
catalytic hydrogenolysis;
参考文献
Journal of the Chemical Society - Series Chemical Communications, , vol. No. 22, p. 1285 - 1286
