3,4,5,7-四甲氧基黄酮合成路线 (共 46 条)
反应条件
sulfuric acid in acetic acid
参考文献
Banerji, Asoke; Goomer, Naresh C.
Synthesis, 1980 , # 11 p. 874 - 875
反应条件
caesium carbonate in acetone T=20°C; 0.166667 h;
参考文献
O'Keefe, B. Michael; Simmons, Nicholas; Martin, Stephen F.
Tetrahedron, 2011 , vol. 67, # 24 p. 4344 - 4351
反应条件
1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in dimethyl sulfoxide T=90°C; 24 h;
参考文献
Barontini, Maurizio; Bernini, Roberta; Crisante, Fernanda; Fabrizi, Giancarlo
Tetrahedron, 2010 , vol. 66, # 32 p. 6047 - 6053
反应条件
sodium methylate in methanol T=0 - 5°C;
参考文献
Bose, Gopal; Mondal, Ejabul; Khan, Abu T; Bordoloi, Manob J.
Tetrahedron Letters, 2001 , vol. 42, # 50 p. 8907 - 8909
反应条件
iodine in dimethyl sulfoxide T=150°C; 0.5 h; Inert atmosphere;
参考文献
Deodhar, Mandar; Wood, Kasey; Black, David Stclair; Kumar, Naresh
Australian Journal of Chemistry, 2012 , vol. 65, # 10 p. 1377 - 1383,7
反应条件
sodium hydride in N,N-dimethyl-formamide T=20°C; 12 h;
参考文献
Matsuda, Hisashi; Morikawa, Toshio; Toguchida, Iwao; Yoshikawa, Masayuki
Chemical and Pharmaceutical Bulletin, 2002 , vol. 50, # 6 p. 788 - 795
反应条件
tetrakis(triphenylphosphine) palladium(0); potassium carbonate in 1,4-dioxane Suzuki coupling; 18 h; Inert atmosphereReflux;
参考文献
Kraus, George A.; Gupta, Vinayak
Organic Letters, 2010 , vol. 12, # 22 p. 5278 - 5280
反应条件
potassium carbonate in acetone 2 h; Heating;
参考文献
Chu, Han-Wei; Wu, Huan-Ting; Lee, Yean-Jang
Tetrahedron, 2004 , vol. 60, # 11 p. 2647 - 2655
反应条件
1: 1.) Lithium diisopropylamide / THF 2: 87 percent / conc. H2SO4 / acetic acid View Scheme
参考文献
Synthesis, , # 11 p. 874 - 875
反应条件
tris(4-bromophenyl)amine; lithium perchlorate in methanol; dichloromethane electrolysis 2 F/mol;
参考文献
Tetrahedron Letters, , vol. 27, # 3 p. 407 - 408