N-乙酰基-3',5'-O-[1,1,3,3-四(异丙基)-1,3-二硅氧烷二基]胞苷合成路线 （共 5 条）
反应条件
1: 70 percent / Ag2O / benzene / Ambient temperature 2: 60 percent / Bu4NF / tetrahydrofuran 3: 70 percent / pyridine View Scheme
参考文献
Reddy; Hanna, Naeem B.; Farooqui, Firdous
Nucleosides and Nucleotides, 1997 , vol. 16, # 7-9 p. 1589 - 1598
反应条件
methylamine in ethanol T=20°C; 0.0833333 h;
参考文献
Drenichev; Kulikova; Bobkov; Tararov; Mikhailov
Synthesis, 2010 , # 22 art. no. P10510SS, p. 3827 - 3834
反应条件
1: 4-N,N-dimethylaminopyridine / acetonitrile / 0.75 h / Ambient temperature 2: n-Bu3SnH, AIBN / toluene / 14 h / 75 °C 3: 1.) TBAF, 2.) NH3 / 1.) THF, 75 deg C, 3 h, 2.) MeOH, room temperature View Scheme
参考文献
Robins; Wilson; Hansske
Journal of the American Chemical Society, 1983 , vol. 105, # 12 p. 4059 - 4065
反应条件
1: 70 percent / Ag2O / benzene / Ambient temperature 2: 60 percent / Bu4NF / tetrahydrofuran 3: 70 percent / pyridine 4: 65 percent / iPr2NEt / tetrahydrofuran View Scheme
参考文献
Reddy; Hanna, Naeem B.; Farooqui, Firdous
Nucleosides and Nucleotides, 1997 , vol. 16, # 7-9 p. 1589 - 1598
反应条件
1: 70 percent / Ag2O / benzene / Ambient temperature 2: 60 percent / Bu4NF / tetrahydrofuran View Scheme
参考文献
Reddy; Hanna, Naeem B.; Farooqui, Firdous
Nucleosides and Nucleotides, 1997 , vol. 16, # 7-9 p. 1589 - 1598
