1: acetoacetic acid methyl ester With sodium hydride
2: ethyl 1-phenylallyl carbonate With (pentamethylcyclopentadienyl)Ru(1,5-cyclooctadiene)Cl; bis(mesityl)ethylenediimine in tetrahydrofuran
T=20°C; 16 h; Title compound not separated from byproducts;
参考文献
Renaud, Jean-Luc; Bruneau, Christian; Demerseman, Bernard
Synlett, 2003 , # 3 p. 408 - 410
bis(η3-allyl-μ-chloropalladium(II)); triphenylphosphine in tetrahydrofuran
T=0°C; 12 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Kawatsura, Motoi; Uozumi, Yasuhiro; Hayashi, Tamio
Chemical Communications, 1998 , # 2 p. 217 - 218