5-[1,1'-联苯]-4-基-2-苯基恶唑合成路线 (共 7 条)
反应条件
iodine in dimethyl sulfoxide
T=100°C;
参考文献
Gao, Qing-He; Fei, Zhuan; Zhu, Yan-Ping; Lian, Mi; Jia, Feng-Cheng; Liu, Mei-Cai; She, Neng-Fang; Wu, An-Xin
Tetrahedron, 2013 , vol. 69, # 1 p. 22 - 28
反应条件
1: With aluminium trichloride in 1,2-dichloro-ethane
T=0 - 20°C; Friedel-Crafts acylation;
2: With trifluorormethanesulfonic acid in 1,2-dichloro-ethane
T=-78 - 20°C; Robinson-Gabriel cyclodehydration;
参考文献
Keni, Manasi; Tepe, Jetze J.
Journal of Organic Chemistry, 2005 , vol. 70, # 10 p. 4211 - 4213
反应条件
indium; acetic acid in acetonitrile
1 h; Inert atmosphereReflux;
参考文献
Lee, Jung June; Kim, Jihye; Jun, Young Moo; Lee, Byung Min; Kim, Byeong Hyo
Tetrahedron, 2009 , vol. 65, # 43 p. 8821 - 8831
参考文献
Hayes et al.
Journal of the American Chemical Society, 1952 , vol. 74, p. 1106
参考文献
Hayes et al.
Journal of the American Chemical Society, 1952 , vol. 74, p. 1106
参考文献
Hayes et al.
Journal of the American Chemical Society, 1952 , vol. 74, p. 1106
反应条件
1: iodine / dimethyl sulfoxide / 100 °C
2: iodine / dimethyl sulfoxide / 100 °C
View Scheme
参考文献
Gao, Qing-He; Fei, Zhuan; Zhu, Yan-Ping; Lian, Mi; Jia, Feng-Cheng; Liu, Mei-Cai; She, Neng-Fang; Wu, An-Xin
Tetrahedron, 2013 , vol. 69, # 1 p. 22 - 28