(-)-B-二异松莰烯基烯丙基硼合成路线 （共 10 条）
反应条件
in diethyl ether T=-100°C; Title compound not separated from byproducts;
参考文献
Tetrahedron Letters, , vol. 41, # 48 p. 9245 - 9249
反应条件
8-hydroxy-quinoline 1) anh. ether, -100 deg C, 1 h, 2) methanol, 25 deg C, 12 h; Yield given. Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 57, # 24 p. 6614 - 6617
反应条件
1: in diethyl ether T=-78°C; 1 h; 2: With dihydrogen peroxide; sodium hydroxide in diethyl ether; water T=25°C; 2 h;
参考文献
Shelke, Anil M.; Rawat, Varun; Suryavanshi, Gurunath; Sudalai, Arumugam
Tetrahedron Asymmetry, 2012 , vol. 23, # 22-23 p. 1534 - 1541
反应条件
in diethyl ether T=-100°C; Title compound not separated from byproducts;
参考文献
Girard; Robins; Villieras; Lebreton
Tetrahedron Letters, 2000 , vol. 41, # 48 p. 9245 - 9249
反应条件
1: in diethyl ether T=-78°C; 3 h; Inert atmosphere; 2: With dihydrogen peroxide; sodium hydroxide in methanol; diethyl ether; water T=-78 - 23°C; Inert atmosphere;
参考文献
Kister, Jeremy; Nuhant, Philippe; Lira, Ricardo; Sorg, Achim; Roush, William R.
Organic Letters, 2011 , vol. 13, # 7 p. 1868 - 1871
反应条件
1: in diethyl ether; dichloromethane; pentane T=-100°C; 2 h; 2: With sodium hydroxide; dihydrogen peroxide in diethyl ether; dichloromethane; pentane T=20°C; 4 h; Title compound not separated from byproducts;
参考文献
Ramachandran, P. Veeraraghavan; Prabhudas, Bodhuri; Chandra, J. Subash; Reddy, M. Venkat Ram
Journal of Organic Chemistry, 2004 , vol. 69, # 19 p. 6294 - 6304
反应条件
1: in diethyl ether
T=-78°C; 3 h; Inert atmosphere;
2: With dihydrogen peroxide; sodium acetate in water
T=0 - 20°C; 0.333333 h;
参考文献
Wang, Jie; Sun, Bing-Feng; Cui, Kai; Lin, Guo-Qiang
Organic Letters, 2012 , vol. 14, # 24 p. 6354 - 6357
反应条件
1: in diethyl ether; dichloromethane
T=-100°C;
2: With sodium hydroxide; dihydrogen peroxide in diethyl ether; dichloromethane; water
Heating; Further stages. Title compound not separated from byproducts.;
参考文献
Klauck, Maggie I.; Patel, Sachin G.; Wiskur, Sheryl L.
Journal of Organic Chemistry, 2012 , vol. 77, # 7 p. 3570 - 3575
反应条件
sodium hydroxide; dihydrogen peroxide
1) Et2O, -100 deg C, 0.5h, 2) MeOH, 3h, reflux; Yield given. Multistep reaction;
参考文献
Hirayama, Lacie C.; Haddad, Terra D.; Oliver, Allen G.; Singaram, Bakthan
Journal of Organic Chemistry, 2012 , vol. 77, # 9 p. 4342 - 4353
反应条件
in diethyl ether
T=-78°C; 3 h; or with B-allyldiisocampheylborane (19), var. α-substituted chiral aldehydes; Product distribution;
参考文献
Brown, Herbert C.; Bhat, Krishna S.; Randad, Ramnarayan S.
Journal of Organic Chemistry, 1989 , vol. 54, # 7 p. 1570 - 1576
