1-苄基-1H-咪唑-5-甲醛合成路线 （共 17 条）
反应条件
manganese(IV) oxide in 1,4-dioxane T=80°C; 6 h;
参考文献
Kokosa, John M.; Szafasz, Richard A.; Tagupa, Eumar
Journal of Organic Chemistry, 1983 , vol. 48, # 20 p. 3605 - 3607
反应条件
in dichloromethane T=-78 - 20°C; 2 - 2.41667 h;
参考文献
Perez, Michel; Lamothe, Marie; Hill, Bridget; Etievant, Chantal
Patent: US2004/204417 A1, 2004 ;
Location in patent: Page 47-48 ;
US 20040204417 A1
反应条件
sodium periodate; K2S2O2(OH)4 in 1,4-dioxane; water T=60°C; 24 h;
参考文献
Cappon, J. J.; Witters, K. D.; Baart, J.; Verdegem, P. J. E.; Hoek, A. C.; et al.
Recueil des Travaux Chimiques des Pays-Bas, 1994 , vol. 113, # 6 p. 318 - 328
反应条件
1: H2 / 10percent Pd on C / ethanol / 2068.6 Torr 2: NaOH / ethanol / 1 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 52, # 13 p. 2714 - 2726
反应条件
selenium(IV) oxide in acetic acid 10 h; Heating;
参考文献
Ranganathan, Darshan; Farooqui, Firdous; Bhattacharyya, Diphti; Mehrotra, Sanjiv; Kesavan, K.
Tetrahedron, 1986 , vol. 42, # 16 p. 4481 - 4492
反应条件
1: aq. NaOH / methanol / 20 °C 2: MnO2 / dioxane / 3 h / 30 - 40 °C View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 53, # 10 p. 1324 - 1326
反应条件
1: 10 percent / Et3N / dimethylformamide / 4 h / Heating 2: 78 percent / MnO2 / dioxane / 6 h / 85 °C View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 4, # 3 p. 482 - 492
反应条件
in acetonitrile T=20 - 60°C; Inert atmosphere;
参考文献
Journal of Medicinal Chemistry, , vol. 52, # 12 p. 3703 - 3715
反应条件
sodium hydroxide; tetrabutylammomium bromide in toluene T=20°C; 4 h;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 54, # 5 p. 706 - 710
反应条件
1: 53 percent / aq. HNO3 / 5 h / 35 - 37 °C 2: 80 percent / MnO2 / dioxane / 6 h / Heating View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 33, # 4 p. 1345 - 1354
