(9ci)-1-甲基-4-硝基-1H-咪唑-5-羧醛合成路线 （共 5 条）
反应条件
manganese(IV) oxide in chloroform
0.5 h; Heating;
参考文献
Shafiee, Abbas; Rastkary, Noushin; Jorjani, Masoumeh; Shafaghi, Bijan
Archiv der Pharmazie (Weinheim, Germany), 2002 , vol. 335, # 2 p. 69 - 76
Title/Abstract Full Text Show Details
Shafiee, Abbas; Rastkary, Noushin; Jorjani, Masoumeh
Arzneimittel-Forschung/Drug Research, 2002 , vol. 52, # 7 p. 537 - 542
反应条件
1.1: SOCl2 / CHCl3 / 1 h / Heating
1.2: HNO3; H2SO4; water / 2 h / 20 °C
1.3: 60 percent / water / propan-2-ol / 24 h / Heating
2.1: 80 percent / MnO2 / CHCl3 / 0.5 h / Heating
View Scheme
参考文献
Shafiee, Abbas; Rastkary, Noushin; Jorjani, Masoumeh
Arzneimittel-Forschung/Drug Research, 2002 , vol. 52, # 7 p. 537 - 542
反应条件
1.1: 85 percent / Raney nickel / ethanol / 3 h / Heating
2.1: SOCl2 / CHCl3 / 1 h / Heating
2.2: HNO3; H2SO4; water / 2 h / 20 °C
2.3: 60 percent / water / propan-2-ol / 24 h / Heating
3.1: 80 percent / MnO2 / CHCl3 / 0.5 h / Heating
View Scheme
参考文献
Shafiee, Abbas; Rastkary, Noushin; Jorjani, Masoumeh
Arzneimittel-Forschung/Drug Research, 2002 , vol. 52, # 7 p. 537 - 542
反应条件
silver perchlorate in water; toluene
2.5 h; Heating;
参考文献
Ostrowski, S.
Polish Journal of Chemistry, 1994 , vol. 68, # 11 p. 2237 - 2248
反应条件
in benzene
8 h; Heating; Title compound not separated from byproducts;
参考文献
Bochwic, Boleslaw; Frankowski, Andrzej; Kuswik, Gabriela; Seliga, Czeslawa
Polish Journal of Chemistry, 1981 , vol. 55, # 5 p. 1055 - 1061
