2-(4-氯苯甲酰)苯甲酸合成路线 （共 35 条）
反应条件
[bmim]Cl*AlCl3 T=60°C; Friedel-Crafts reaction; 4 h;
参考文献
Mohile, Swapnil S.; Potdar, Mahesh K.; Salunkhe, Manikrao M.
Journal of Chemical Research - Part S, 2003 , # 10 p. 650 - 651
反应条件
palladium (II) trifluoroacetate; silver carbonate in ethylene glycol dimethyl ether T=150°C; 24 h; Sealed tube; chemoselective reaction;
参考文献
Miao, Jinmin; Ge, Haibo
Organic Letters, 2013 , vol. 15, # 12 p. 2930 - 2933
反应条件
sodium hydroxide; potassium permanganate in pyridine
参考文献
Chemische Berichte, , vol. 101, p. 2660 - 2664
反应条件
1: SOCl2 2: aq. KMnO4, NaOH / pyridine View Scheme
参考文献
Chemische Berichte, , vol. 101, p. 2660 - 2664
反应条件
1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 0 - 20 °C / |Inert atmosphere 2: potassium carbonate / water; ethyl acetate / 4 h / 0 °C 3: palladium diacetate; boron trifluoride diethyl etherate; tert.-butylhydroperoxide; water / dimethyl sulfoxide; 1,4-dioxane / 130 °C 4: hydrogenchloride; water / dimethyl sulfoxide; 1,4-dioxane / 6 h / 100 °C View Scheme
参考文献
Chemical Communications, , vol. 49, # 82 p. 9464 - 9466
反应条件
1: potassium carbonate / water; ethyl acetate / 4 h / 0 °C 2: palladium diacetate; boron trifluoride diethyl etherate; tert.-butylhydroperoxide; water / dimethyl sulfoxide; 1,4-dioxane / 130 °C 3: hydrogenchloride; water / dimethyl sulfoxide; 1,4-dioxane / 6 h / 100 °C View Scheme
参考文献
Chemical Communications, , vol. 49, # 82 p. 9464 - 9466
反应条件
hydrogenchloride Heatingovernight; Yield given;
参考文献
Journal of Organic Chemistry, , vol. 47, # 8 p. 1585 - 1587
反应条件
1: 1.) BuLi / 1.) THF, -45 deg C, 2.) -100 deg C 2: 5percent aq. HCl / Heating; overnight View Scheme
参考文献
Journal of Organic Chemistry, , vol. 47, # 8 p. 1585 - 1587
反应条件
1: 1.) BuLi / 1.) THF, -45 deg C, 2.) -100 deg C 2: 5percent aq. HCl / Heating; overnight View Scheme
参考文献
Journal of Organic Chemistry, , vol. 47, # 8 p. 1585 - 1587
反应条件
1: palladium diacetate; boron trifluoride diethyl etherate; tert.-butylhydroperoxide; water / dimethyl sulfoxide; 1,4-dioxane / 130 °C 2: hydrogenchloride; water / dimethyl sulfoxide; 1,4-dioxane / 6 h / 100 °C View Scheme
参考文献
Chemical Communications, , vol. 49, # 82 p. 9464 - 9466
