1,2-二(2-羟基苯基)-1,2-乙烷二酮合成路线 （共 11 条）
反应条件
CuSO4‵5H2O; triethylamine in water; acetonitrile
T=85°C; 0.166667 h;
参考文献
Zhang, Xiang; Fu, Jie; Zhan, Tian-Guang; Dai, Liyan; Chen, Yingqi; Zhao, Xin
Tetrahedron Letters, 2013 , vol. 54, # 37 p. 5039 - 5042
反应条件
AlCl3, aluminium chloride in dichloromethane
T=20°C; 3 h;
参考文献
Seo, Min-Seob; Lee, Ansoo; Kim, Hyunwoo
Organic Letters, 2014 , vol. 16, # 11 p. 2950 - 2953
反应条件
aluminium trichloride; nitrobenzene
T=55°C;
参考文献
Kuhn; Birkofer; Moeller
Chemische Berichte, 1943 , vol. 76, p. 900,903
反应条件
1: aq. NaCN / ethanol
2: 65 percent aq. HNO3 / 0.75 h / Heating
View Scheme
参考文献
Tarassoli, Abbas; Shushizadeh, Mohammad Reza
Phosphorus, Sulfur and Silicon and the Related Elements, 2003 , vol. 178, # 4 p. 803 - 809
反应条件
1: 1,8-diazabicyclo[5.4.0]undec-7-ene; thiamine hydrochloride / dimethyl sulfoxide / 5 h / 60 °C / |Inert atmosphere
2: triethylamine; CuSO4‵5H2O / acetonitrile; water / 0.17 h / 85 °C
View Scheme
参考文献
Zhang, Xiang; Fu, Jie; Zhan, Tian-Guang; Dai, Liyan; Chen, Yingqi; Zhao, Xin
Tetrahedron Letters, 2013 , vol. 54, # 37 p. 5039 - 5042
反应条件
sulfuric acid; acetic acid
参考文献
Farbenfabr. Bayer
Patent: DE875195 , 1944 ;
反应条件
nitric acid
0.75 h; Heating;
参考文献
Tarassoli, Abbas; Shushizadeh, Mohammad Reza
Phosphorus, Sulfur and Silicon and the Related Elements, 2003 , vol. 178, # 4 p. 803 - 809
反应条件
1: KCN; aqueous ethanol / Beim Erwaermen des Reaktionsprodukts in Aethanol mit Fehling'scher Loesung
2: acetic acid; aqueous H2SO4
View Scheme
参考文献
Farbenfabr. Bayer
Patent: DE875195 , 1944 ;
反应条件
in ethanol
0.5 h; Heating;
参考文献
Tarassoli, Abbas; Shushizadeh, Mohammad Reza
Phosphorus, Sulfur and Silicon and the Related Elements, 2003 , vol. 178, # 4 p. 803 - 809
反应条件
bromine; acetic acid
参考文献
Kuhn; Birkofer; Moeller
Chemische Berichte, 1943 , vol. 76, p. 900,903
Full Text Show Details
Schales; Suthon
Archives of Biochemistry, 1946 , vol. 11, p. 397,398
