1-甲基-2-氧代-1,2-二氢-3-吡啶甲酰氯合成路线 （共 5 条）
反应条件
thionyl chloride
1.5 h; Heating;
参考文献
Deady, Leslie W.
Australian Journal of Chemistry, 1985 , vol. 38, # 4 p. 637 - 641
反应条件
1: KOH / H2O; methanol / Heating
2: SOCl2 / toluene / 80 °C
View Scheme
参考文献
Masu, Hyuma; Ohmori, Ken; Kishikawa, Keiki; Yamamoto, Makoto; Yamaguchi, Kentaro; Kohmoto, Shigeo
Bulletin of the Chemical Society of Japan, 2005 , vol. 78, # 6 p. 1127 - 1131
参考文献
Deady, Leslie W.
Australian Journal of Chemistry, 1985 , vol. 38, # 4 p. 637 - 641
反应条件
in benzene
0.166667 h; Ambient temperature;
参考文献
Duong, Thach; Prager, Rolf H.; Were, Stephen T.
Australian Journal of Chemistry, 1983 , vol. 36, # 7 p. 1431 - 1440
反应条件
1: AlCl3 / 6 h / Heating
2: 70 percent / NaBH4 / ethanol / 0.5 h
3: 70 percent / sodium azide, 98percent H2SO4 / CHCl3 / a) RT, overnight, b) 50 deg C, 1 h
View Scheme
参考文献
Duong, Thach; Prager, Rolf H.; Were, Stephen T.
Australian Journal of Chemistry, 1983 , vol. 36, # 7 p. 1431 - 1440
