3-氨基-5-乙酰基亚氨基二苄合成路线 （共 6 条）
反应条件
potassium hydroxide in propan-1-ol 5 h; Heating;
参考文献
Skoldinov, A. P.; Gritsenko, A. N.; Wunderlich, H.; Stark, A.; Carstens, E.; Loman, D.
Pharmaceutical Chemistry Journal, 1990 , vol. 24, # 12 p. 924 - 927
Khimiko-Farmatsevticheskii Zhurnal, 1990 , vol. 24, # 12 p. 51 - 53
反应条件
1: 85 percent / isoamyl nitrite, CuCl2 / acetonitrile / Ambient temperature 2: 95 percent / KOH / methanol / Heating View Scheme
参考文献
Csende, Ferenc; Hosztafi, Sandor
Advanced Synthesis and Catalysis, 1997 , vol. 339, # 6 p. 587 - 589
反应条件
copper dichloride; isopentyl nitrite in acetonitrile Ambient temperature;
参考文献
Advanced Synthesis and Catalysis, , vol. 339, # 6 p. 587 - 589
反应条件
isopentyl nitrite in N,N-dimethyl-formamide
Ambient temperature;
参考文献
Csende, Ferenc; Hosztafi, Sandor
Advanced Synthesis and Catalysis, 1997 , vol. 339, # 6 p. 587 - 589
反应条件
isopentyl nitrite
1) r.t., 20 min, 2) reflux, 2 h;
参考文献
Csende, Ferenc; Hosztafi, Sandor
Advanced Synthesis and Catalysis, 1997 , vol. 339, # 6 p. 587 - 589
反应条件
1: 98 percent / KOH / propan-1-ol / 5 h / Heating
2: 91 percent / 20percent aq. KOH / acetone / 1 h / Heating
3: 97 percent / toluene / 2 h / Heating
4: 76 percent / toluene; H2O / 1.5 h / Heating
View Scheme
参考文献
Skoldinov, A. P.; Gritsenko, A. N.; Wunderlich, H.; Stark, A.; Carstens, E.; Loman, D.
Pharmaceutical Chemistry Journal, 1990 , vol. 24, # 12 p. 924 - 927
Khimiko-Farmatsevticheskii Zhurnal, 1990 , vol. 24, # 12 p. 51 - 53
