1-[2-(甲基硫代)-5-嘧啶]-乙酮合成路线 （共 6 条）
反应条件
sodium tetrahydroborate in isopropyl alcohol 0.5 h;
参考文献
Sandosham, Jessie; Benneche, Tore; Moeller, Bjoerg; Undheim, Kjell
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1988 , vol. 42, # 7 p. 455 - 461
反应条件
MnI2 in tetrahydrofuran; diethyl ether
T=-80°C; 4 h;
参考文献
Arukwe, Joseph; Undheim, Kjell
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1986 , vol. 40, # 9 p. 764 - 767
反应条件
bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran
2 h; Heating;
参考文献
Arukwe, Joseph; Benneche, Tore; Undheim, Kjell
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 255 - 259
反应条件
potassium tert-butylate in acetone; tert-butyl alcohol
24 h; Ambient temperature;
参考文献
Benneche,Tore; Undheim,Kjell
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1982 , vol. 36, # 8 p. 529 - 532
反应条件
phosphorus pentachloride in benzene
3 h; Heating;
参考文献
Benneche, Tore; Undheim, Kjell
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1983 , vol. 37, # 3 p. 235 - 240
反应条件
1: 56 percent / PCl5 / benzene / 3 h / Heating
2: 8 percent / t-BuOK / dimethylformamide / 48 h / Ambient temperature
View Scheme
参考文献
Benneche, Tore; Undheim, Kjell
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1983 , vol. 37, # 3 p. 235 - 240
