2,5-二(4-甲氧基苯基)-1,3,4-恶二唑合成路线 (共 13 条)
反应条件
t-BuOI; carbonic acid dimethyl ester
T=20°C; 0.25 h;
参考文献
Singh, Sushma; Sharma, Laxmi K.; Saraswat, Apoorv; Siddiqui, Ibadur R.; Singh, Rana K. Pal
Research on Chemical Intermediates, 2014 , vol. 40, # 3 p. 947 - 960
反应条件
zirconium tetrachloride in dichloromethane
T=20°C; 2.5 h;
参考文献
Sharma; Begum, Asra; Rakesh; Krishna, Palakodety Radha
Synthetic Communications, 2004 , vol. 34, # 13 p. 2387 - 2391
反应条件
hydraziniumdihydrochloride; phosphoric acid; trichlorophosphate in water
T=140°C; Condensation; 2 h;
参考文献
Bentiss, Fouad; Lagrenee, Michel
Journal of Heterocyclic Chemistry, 1999 , vol. 36, # 4 p. 1029 - 1032
反应条件
trichloroisocyanuric acid in ethanol
T=20°C; 0.5 h;
参考文献
Pore; Mahadik; Desai
Synthetic Communications, 2008 , vol. 38, # 18 p. 3121 - 3128
反应条件
copper(l) iodide; 1,10-phenanthroline; caesium carbonate in dimethyl sulfoxide
T=100°C; 4 h; Inert atmosphere;
参考文献
Kawano, Tsuyoshi; Yoshizumi, Tomoki; Hirano, Koji; Satoh, Tetsuya; Miura, Masahiro
Organic Letters, 2009 , vol. 11, # 14 p. 3072 - 3075
反应条件
1: With hydrazine hydrate in tetrahydrofuran
Heating;
2: With PPA in tetrahydrofuran
T=130°C; 3.5 h;
参考文献
Park, Yong-Dae; Kim, Jeum-Jong; Chung, Hyun-A; Kweon, Deok-Heon; Cho, Su-Dong; Lee, Sang-Gyeong; Yoon, Yong-Jin
Synthesis, 2003 , # 4 p. 560 - 564
反应条件
bis-[(trifluoroacetoxy)iodo]benzene in dimethyl sulfoxide
T=20°C; 0.166667 h;
参考文献
Shang, Zhenhua; Reiner, John; Chang, Junbiao; Zhao, Kang
Tetrahedron Letters, 2005 , vol. 46, # 15 p. 2701 - 2704
反应条件
1,4-diaza-bicyclo[2.2.2]octane; tert.-butylhydroperoxide; tetra-(n-butyl)ammonium iodide; potassium carbonate in methanol; hexane
T=20°C; 4 h;
参考文献
Gao, Peng; Wei, Yunyang
Journal of Chemical Research, 2013 , vol. 37, # 8 p. 506 - 510
反应条件
trichlorophosphate in acetonitrile
2 h; Heating;
参考文献
Tashtoush, Hasan; Al-Talib, Mahmoud; Odeh, Nedal
Liebigs Annalen der Chemie, 1992 , # 3 p. 291 - 292
参考文献
Reddy, P. S. N.; Reddy, P. Pratap
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1987 , vol. 26, # 1-12 p. 890 - 891