2,3,4-三-O-乙酰基-1-硫代-β-L-岩藻糖苷甲酯合成路线 （共 9 条）
反应条件
trimethylsilyl trifluoromethanesulfonate in dichloromethane T=20°C; 15 h;
参考文献
Matwiejuk, Martin; Thiem, Joachim
European Journal of Organic Chemistry, 2011 , # 29 p. 5860 - 5878
反应条件
tin(IV) chloride in 1,2-dichloro-ethane T=20°C; 4 h;
参考文献
Carbohydrate Research, , vol. 201, # 1 p. 31 - 50
反应条件
N-ethyl-N,N-diisopropylamine in dichloromethane 1 h;
参考文献
Jain; Matta
Carbohydrate research, 1990 , vol. 208, p. 51 - 58
反应条件
1: 98 percent / I2 / 0.25 h / 20 °C 2: I2; HMDS / CH2Cl2 / 1.5 h / 20 °C 3: CH2Cl2 / 20 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 69, # 22 p. 7758 - 7760
反应条件
1: I2; HMDS / CH2Cl2 / 1.5 h / 20 °C 2: CH2Cl2 / 20 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 69, # 22 p. 7758 - 7760
反应条件
in dichloromethane T=20°C;
参考文献
Journal of Organic Chemistry, , vol. 69, # 22 p. 7758 - 7760
反应条件
1: acetone / 18 h / Ambient temperature 2: NaOAc / 100 °C View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 55, # 11 p. 3667 - 3668
反应条件
sodium acetate T=100°C; Yield given;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 55, # 11 p. 3667 - 3668
反应条件
1: MeOH, NaOMe / 4 h / 20 °C 2: 1.) NaH / 1.) DMF, 30 min, 20 deg C 2.) DMF, 16 h, 20 deg C View Scheme
参考文献
Yamazaki, Fumito; Sato, Susumu; Nukada, Tomoo; Ito, Yukishige; Ogawa, Tomoya
Carbohydrate Research, 1990 , vol. 201, # 1 p. 31 - 50
