2-(1-萘基)-5-苯基噁唑合成路线 (共 6 条)
反应条件
copper(l) iodide; potassium carbonate; palladium diacetate in N,N-dimethyl-formamide T=150°C; 0.25 h; microwave irradiation;
参考文献
Journal of Organic Chemistry, , vol. 73, # 8 p. 3278 - 3280
反应条件
pyridine; oxygen; potassium carbonate; copper(I) bromide in toluene T=80°C; P=760.051 Torr; 16 h; Schlenk technique;
参考文献
Xu, Zejun; Zhang, Chun; Jiao, Ning
Angewandte Chemie - International Edition, 2012 , vol. 51, # 45 p. 11367 - 11370
Angew. Chem.
反应条件
1: 1-naphthylCHNOH With trifluorormethanesulfonic acid; silica gel in toluene T=50°C; 0.5 h; 2: phenylacetylene in toluene T=70°C; 3.5 h; 3: With CuCl2·2H2O; lithium chloride monohydrate; oxygen; 2,3-dicyano-5,6-dichloro-p-benzoquinone in 1,4-dioxane; propan-1-ol; toluene T=60°C; P=9750.98 Torr; 4 h;
参考文献
Yuan, Shizhen; Li, Zhen; Xu, Ling
Journal of Heterocyclic Chemistry, 2013 , vol. 50, # 6 p. 1405 - 1409
反应条件
bis-triphenylphosphine-palladium(II) chloride; n-butyllithium in tetrahydrofuran; diethyl ether; hexane 1 h; Heating;
参考文献
Anderson, Benjamin A.; Harn, Nancy K.
Synthesis, 1996 , # 5 p. 583 - 585
参考文献
Journal of the Chemical Society, , vol. 101, p. 1313
反应条件
1: KOH-solution 2: concentrated sulfuric acid View Scheme
参考文献
Journal of the Chemical Society, , vol. 101, p. 1313