双［4-(1,1-二甲基乙基)苯基］碘鎓与三氟甲磺酸的盐合成路线 （共 6 条）
反应条件
iodine; 3-chloro-benzenecarboperoxoic acid in dichloromethane T=20°C; 0.166667 h;
参考文献
Jalalian, Nazli; Petersen, Tue B.; Olofsson, Berit
Chemistry--A European Journal, 2012 , vol. 18, # 44 p. 14140 - 14149,10
反应条件
1: trifluoromethylsulfonic anhydride With urea hydrogen peroxide addition compound in dichloromethane; 2,2,2-trifluoroethanol T=0°C; 0.5 h; 2: 1-tert-butyl-4-iodobenzene in dichloromethane; 2,2,2-trifluoroethanol T=0°C; 3: tert-butyl benzene in dichloromethane; 2,2,2-trifluoroethanol T=0 - 20°C;
参考文献
Merritt, Eleanor A.; Malmgren, Joel; Klinke, Felix J.; Olofsson, Berit
Synlett, 2009 , # 14 p. 2277 - 2280
反应条件
[(2-phenylpyridine(-H))2IrIII(2,2′-bipyridine)]PF6; cyclohexa-1,4-diene in acetonitrile T=20°C; 2 h; Inert atmosphereIrradiation; Reagent/catalystTimeTemperature;
参考文献
Tobisu, Mamoru; Furukawa, Takayuki; Chatani, Naoto
Chemistry Letters, 2013 , vol. 42, # 10 p. 1203 - 1205
反应条件
sodium hydroxide in water T=20 - 50°C; 3 h;
参考文献
Organic Letters, , vol. 15, # 23 p. 6070 - 6073
反应条件
1: phenol With potassium tert-butylate in tetrahydrofuran
T=0°C; 0.25 h;
2: bis(4-tertbutylphenyl)iodonium trifluoromethanesulfonate in tetrahydrofuran
T=40°C; 5 h;
参考文献
Jalalian, Nazli; Petersen, Tue B.; Olofsson, Berit
Chemistry--A European Journal, 2012 , vol. 18, # 44 p. 14140 - 14149,10
反应条件
sodium hydroxide in water
T=20 - 50°C; 3 h;
参考文献
Lindstedt, Erik; Ghosh, Raju; Olofsson, Berit
Organic Letters, 2013 , vol. 15, # 23 p. 6070 - 6073
