3-硝基-6,7-二氢-5-氢-环戊烷[B]吡啶合成路线 （共 7 条）
反应条件
ammonia in methanol
T=70°C; 3 h; Inert atmosphere;
参考文献
GRÜNENTHAL GMBH; FRANK, Robert; CHRISTOPH, Thomas; LESCH, Bernhard; LEE, Jeewoo
Patent: WO2013/13816 A1, 2013 ;
Location in patent: Page/Page column 72 ;
反应条件
ammonia in methanol
T=70°C; 3 h;
参考文献
Tohda; Eiraku; Nakagawa; Usami; Ariga; Kawashima; Tani; Watanabe; Mori
Bulletin of the Chemical Society of Japan, 1990 , vol. 63, # 10 p. 2820 - 2827
反应条件
ammonia in methanol
T=70°C; 3 h;
参考文献
Tohda; Eiraku; Nakagawa; Usami; Ariga; Kawashima; Tani; Watanabe; Mori
Bulletin of the Chemical Society of Japan, 1990 , vol. 63, # 10 p. 2820 - 2827
反应条件
in nitrobenzene
T=210°C; 0.5 h;
参考文献
Frissen, A. E.; Marcelis, A. T. M.; Geurtsen, G.; Bie, D. A. de; Plas, H. C. van der
Tetrahedron, 1989 , vol. 45, # 16 p. 5151 - 5162
反应条件
in ethanol
T=70°C; 2 h;
参考文献
Charushin, Valery N.; van der Plas, Henk C.
Tetrahedron Letters, 1982 , vol. 23, # 38 p. 3965 - 3968
反应条件
in ethanol
2 h; Heating;
参考文献
Marcelis, Antonius T. M.; Plas, Henk C. van der
Tetrahedron, 1989 , vol. 45, # 9 p. 2693 - 2702
反应条件
palladium on activated charcoal; hydrogen in methanol
T=20°C; 2 h;
参考文献
Gruenenthal GmbH; FRANK, Robert; CHRISTOPH, Thomas; LESCH, Bernhard; LEE, Jeewoo
Patent: US2013/29995 A1, 2013 ;
Location in patent: Paragraph 0364-0365 ;
US 20130029995 A1
