5-碘-1-(2,3,5-三-O-乙酰基-beta-D-阿拉伯呋喃糖基)-2,4(1H,3H)-嘧啶二酮合成路线 (共 3 条)
反应条件
1: triethylamine; copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide 2: tetrabutyl ammonium fluoride / acetonitrile 3: sodium hydroxide / ethanol View Scheme
参考文献
Dojahn, Claudine M.; Hesse, Marlen; Arenz, Christoph
Chemical Communications, 2013 , vol. 49, # 30 p. 3128 - 3130
反应条件
sodium methylate in methanol 1 h; Ambient temperature;
参考文献
Asakura, Jun-ichi; Robins, Morris J.
Journal of Organic Chemistry, 1990 , vol. 55, # 16 p. 4928 - 4933
反应条件
sodium methylate in methanol T=20°C; 0.5 h;
参考文献
Lin, Kun-I.; Chiang, Li-Wu; Wu, Chien-Hung; Chen, Shao-Wei; Yu, Chung-Shan
Journal of the Chinese Chemical Society, 2007 , vol. 54, # 2 p. 563 - 568