1-(1-甲氧基异丙氧基)戊-2-炔合成路线 (共 3 条)
反应条件
water; Amberlyst.(R). 15 T=22°C; 1.5 h; Inert atmosphere; Product distribution / selectivity;
参考文献
Bonrath, Werner; Pace, Francesco; Fischesser, Jocelyn; Witzgall, Konrad
Patent: US2012/197046 A1, 2012 ;
Location in patent: Page/Page column 8 ;
反应条件
1: 3-(2-methoxypropan-2-yloxy)prop-1-yne With ammonia; lithium; isoprene
T=-37°C; 1.5 h;
2: ethyl iodide 1.5 h;
参考文献
Bonrath, Werner; Pace, Francesco; Fischesser, Jocelyn; Witzgall, Konrad
Patent: US2012/197046 A1, 2012 ;
Location in patent: Page/Page column 7 ;
反应条件
1: 3-(2-methoxypropan-2-yloxy)prop-1-yne With piperylene; ammonia; lithium
T=-37°C; 1.5 h;
2: ethyl bromide 1.5 h; Product distribution / selectivity;
参考文献
Bonrath, Werner; Pace, Francesco; Fischesser, Jocelyn; Witzgall, Konrad
Patent: US2012/197046 A1, 2012 ;
Location in patent: Page/Page column 7 ;