2-(4-甲氧基苯基)-5-苯基-1,3,4-恶二唑合成路线 （共 37 条）
反应条件
in 1,3,5-trimethyl-benzene
T=160 - 170°C; 1 h;
参考文献
Uher, Michal; Foltin, Jozef; Povazanec, Frantisek; Kovac, Jaroslav
Collection of Czechoslovak Chemical Communications, 1981 , vol. 46, # 6 p. 1492 - 1494
反应条件
1: aq. NaOH / diethyl ether
2: butane-1,2-diol, nPr3N
View Scheme
参考文献
Eilingsfeld,H.
Chemische Berichte, 1965 , vol. 98, p. 1308 - 1321
反应条件
tri(n-propyl)amine; (2R,3R)-(-)butanediol
参考文献
Eilingsfeld,H.
Chemische Berichte, 1965 , vol. 98, p. 1308 - 1321
参考文献
Shawali,A.S.; Fahmi,A.-G.A.
Journal of Heterocyclic Chemistry, 1977 , vol. 14, p. 1089 - 1092
反应条件
1: NaNO2; aqueous HCl
View Scheme
参考文献
Grekow et al.
Zhurnal Obshchei Khimii, 1959 , vol. 29, p. 3054,3055; engl. Ausg. S. 3020, 3021
反应条件
1: POCl3
3: NaNO2; aqueous HCl
View Scheme
参考文献
Grekow et al.
Zhurnal Obshchei Khimii, 1959 , vol. 29, p. 3054,3055; engl. Ausg. S. 3020, 3021
反应条件
2: NaNO2; aqueous HCl
View Scheme
参考文献
Grekow et al.
Zhurnal Obshchei Khimii, 1959 , vol. 29, p. 3054,3055; engl. Ausg. S. 3020, 3021
反应条件
1: hydrazine
2: pyridine / Heating
3: trichlorophosphate / 10 h / Reflux
View Scheme
参考文献
Gierczyk, Blazej; Zalas, MacIej; Kazmierczak, Marcin; Grajewski, Jakub; Pankiewicz, Radoslaw; Wyrzykiewicz, Bozena
Magnetic Resonance in Chemistry, 2011 , vol. 49, # 10 p. 648 - 654
参考文献
Huisgen,R. et al.
Chemische Berichte, 1960 , vol. 93, p. 2106 - 2124
反应条件
sodium hydroxide; tri-n-butylammonium bromide
1) CH2Cl2, 25 deg C, 3 h, 2)80 - 130 deg C; Yield given. Multistep reaction;
参考文献
Osipova, T. F.; Koldobskii, G. I.; Ostrovskii, V. A.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, p. 2248 - 2252
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 11 p. 2468 - 2473
