2-(4-甲氧基苯基)-5-苯基-1,3,4-恶二唑合成路线 (共 37 条)
反应条件
tert.-butylhydroperoxide; tetra-(n-butyl)ammonium iodide; potassium carbonate in water; ethyl acetate
T=60°C; 1 h;
参考文献
Gao, Peng; Wei, Yunyang
Journal of Chemical Research, 2013 , vol. 37, # 8 p. 506 - 510
反应条件
1: in N,N-dimethyl-formamide
T=60°C; Inert atmosphere;
2: With N-ethyl-N,N-diisopropylamine; Eosin in N,N-dimethyl-formamide
T=20°C; 12 h; IrradiationInert atmosphere;
参考文献
Yadav, Arvind K.; Yadav, Lal Dhar S.
Tetrahedron Letters, 2014 , vol. 55, # 13 p. 2065 - 2069
反应条件
1: in N,N-dimethyl-formamide
T=60°C; Inert atmosphere;
2: With N-ethyl-N,N-diisopropylamine; Eosin in N,N-dimethyl-formamide
T=20°C; 12 h; IrradiationInert atmosphere;
参考文献
Yadav, Arvind K.; Yadav, Lal Dhar S.
Tetrahedron Letters, 2014 , vol. 55, # 13 p. 2065 - 2069
反应条件
trichlorophosphate
T=120°C; 7 h;
参考文献
Chiu, Yi-Hong; Liu, Jui-Hsiang
Journal of Polymer Science, Part A: Polymer Chemistry, 2010 , vol. 48, # 15 p. 3368 - 3374
反应条件
oxygen; copper(II) bis(trifluoromethanesulfonate); caesium carbonate in N,N-dimethyl-formamide
T=110°C; 10 h;
参考文献
Guin, Srimanta; Ghosh, Tuhin; Rout, Saroj Kumar; Banerjee, Arghya; Patel, Bhisma K.
Organic Letters, 2011 , vol. 13, # 22 p. 5976 - 5979
反应条件
sodium carbonate; tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide
T=85°C; Suzuki coupling; 3 h;
参考文献
Vachal, Petr; Toth, Leslie M.
Tetrahedron Letters, 2004 , vol. 45, # 38 p. 7157 - 7161
反应条件
potassium permanganate in water; acetone
0.133333 h; microwave irradiation;
参考文献
Rostamizadeh, Shahnaz; Housaini, S.A. Ghasem
Tetrahedron Letters, 2004 , vol. 45, # 47 p. 8753 - 8756
反应条件
copper(l) iodide; 1,10-phenanthroline; caesium carbonate in dimethyl sulfoxide
T=100°C; 4 h; Inert atmosphere;
参考文献
Kawano, Tsuyoshi; Yoshizumi, Tomoki; Hirano, Koji; Satoh, Tetsuya; Miura, Masahiro
Organic Letters, 2009 , vol. 11, # 14 p. 3072 - 3075
反应条件
1: With N-ethyl-N,N-diisopropylamine; HATU in tetrahydrofuran
T=20°C; 0.75 h;
2: With Burgess Reagent in tetrahydrofuran
T=20°C;
参考文献
Li, Changkun; Dickson, Hamilton D.
Tetrahedron Letters, 2009 , vol. 50, # 47 p. 6435 - 6439
反应条件
bis-[(trifluoroacetoxy)iodo]benzene in dimethyl sulfoxide
T=20°C; 0.166667 h;
参考文献
Shang, Zhenhua; Reiner, John; Chang, Junbiao; Zhao, Kang
Tetrahedron Letters, 2005 , vol. 46, # 15 p. 2701 - 2704