1: aniline With Fe(HSO4)3; silica gel; sodium nitrite in water Green chemistry; 2: β-naphthol in water T=20°C; 0.166667 h; Green chemistry; regioselective reaction;
参考文献
Rahimizadeh, Mohammad; Eshghi, Hossein; Shiri, Ali; Ghadamyari, Zohreh; Matin, Maryam M.; Oroojalian, Fatemeh; Pordeli, Parvaneh
Journal of the Korean Chemical Society, 2012 , vol. 56, # 6 p. 716 - 719
1: aniline With hydrogenchloride in water T=0 - 5°C; 0.0833333 h; 2: With 1-(4-(nitrosooxy)butyl)-3-methylimidazolium chloride in water T=0 - 5°C; 0.416667 h; 3: β-naphthol With sodium hydroxide in water T=0°C; 0.416667 h;
参考文献
Valizadeh, Hassan; Shomali, Ashkan
Dyes and Pigments, 2012 , vol. 92, # 3 p. 1138 - 1143
Butler, Richard N.; O'Shea, Paul D.; Shelly, Declan P.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 1039 - 1042
Journal of Organic Chemistry, , vol. 51, # 1 p. 88 - 92
→
反应条件
aniline in acetonitrile added aniline to a soln. of Ru-complex; stirred for 30 min at room temp.; evapd. to dryness; extracted with ice-cold water; filtrated; added β-naphthol with stirring over a period of 15 min; sepd.; recrystd. from methanol; dried residue obtained after water extraction; dissolved in CH2Cl2; added hexane; filtered; dried in vacuo; elem. anal.;
参考文献
Deb, Alok Kumar; Goswami, Sreebrata
Polyhedron, 1991 , vol. 10, p. 1799 - 1802
