2,3-二氢-3-甲基-1,2-苯异噻唑 1,1-二氧化物合成路线 （共 4 条）
反应条件
[bis(acetoxy)iodo]benzene; magnesium oxide; dirhodium tetraacetate in dichloromethane
Heating;
参考文献
Fruit, Corinne; Mueller, Paul
Helvetica Chimica Acta, 2004 , vol. 87, # 7 p. 1607 - 1615
反应条件
sodium tetrahydroborate in diethyl ether; ethanol
24 h; Ambient temperature;
参考文献
Teeninga, Herman; Engberts, Jan B. F. N.
Journal of Organic Chemistry, 1983 , vol. 48, # 4 p. 537 - 542
反应条件
1: 73 percent / n-BuLi / hexane; tetrahydrofuran / 1 h / 0 °C
2: 98 percent / TFA / methoxybenzene; ethyl acetate / 24 h / 0 °C
3: 65 percent / PhI(OAc)2; MgO / [Rh2(OAc)4] / CH2Cl2 / Heating
View Scheme
参考文献
Fruit, Corinne; Mueller, Paul
Helvetica Chimica Acta, 2004 , vol. 87, # 7 p. 1607 - 1615
反应条件
1: 98 percent / TFA / methoxybenzene; ethyl acetate / 24 h / 0 °C
2: 65 percent / PhI(OAc)2; MgO / [Rh2(OAc)4] / CH2Cl2 / Heating
View Scheme
参考文献
Fruit, Corinne; Mueller, Paul
Helvetica Chimica Acta, 2004 , vol. 87, # 7 p. 1607 - 1615
