2-脱氧链霉胺,二氢溴酸盐合成路线 （共 3 条）
反应条件
water; hydrogen bromide
T=100°C; 40 h; Heating / reflux;
参考文献
ISIS Pharmaceuticals, Inc.
Patent: US6759523 B2, 2004 ;
Location in patent: Page column 18-19 ;
反应条件
hydrogen bromide
T=100°C; 120 h;
参考文献
Pinsetta, Flavio Roberto; Kawano, Daniel Fabio; De Carvalho, Marcelo Rodrigues; De Oliveira, Jose Antonio A.; Corrado, Alexandre P.; Hyppolito, Miguel Angelo; Carvalho, Ivone
Carbohydrate Research, 2013 , vol. 373, p. 97 - 102
反应条件
1: CF3CON3; CuSO4; Et3N / acetonitrile
2: DMAP / pyridine
View Scheme
参考文献
Pinsetta, Flavio Roberto; Kawano, Daniel Fabio; De Carvalho, Marcelo Rodrigues; De Oliveira, Jose Antonio A.; Corrado, Alexandre P.; Hyppolito, Miguel Angelo; Carvalho, Ivone
Carbohydrate Research, 2013 , vol. 373, p. 97 - 102
