N-乙酰-L-酪氨酸乙酯合成路线 (共 17 条)
反应条件
α-chymotryosin; triethylamine in water; isopropyl alcohol T=30°C; 2 h; pH 9.5; various content of water; other solvents, other aliphatic alcohols; Product distribution;
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 54, # 1 p. 266 - 276
反应条件
sodium chloride; calcium chloride; α-chymotrypsin T=25°C; Condensation; pH=8.0; Product distribution; Further Variations:Temperatures;
参考文献
Wehofsky, Nicole; Haensler, Marion; Kirbach, Sebastian W.; Wissmann, Johannes-Dieter; Bordusa, Frank
Tetrahedron Asymmetry, 2000 , vol. 11, # 11 p. 2421 - 2428
反应条件
1: 2.) 100 mM ascorbic acid / 1.) polyphenol oxidase / 1.) chloroform, 25 deg C, 4 h; 2.) water 2: 3 N NaOH / 3 h / 65 °C View Scheme
参考文献
Kazandjian, Rafi Z.; Klibanov, Alexander M.
Journal of the American Chemical Society, 1985 , vol. 107, # 19 p. 5448 - 5450
参考文献
Kaufman; Neurath
Journal of Biological Chemistry, 1949 , vol. 180, p. 181
反应条件
1: 4-(N,N-dimethlyamino)pyridine; triethylamine / dichloromethane / Inert atmosphere 2: [Ni0(1,5-cyclooctadiene)2]; methyl dimethoxy silane; tri-cyclo-hexyl-phosphine / toluene / 12 h / 80 °C / Inert atmosphere View Scheme
参考文献
Tobisu, Mamoru; Yamakawa, Ken; Shimasaki, Toshiaki; Chatani, Naoto
Chemical Communications, 2011 , vol. 47, # 10 p. 2946 - 2948
反应条件
Rhizobium meliloti cyclosophoraoses T=60°C; KineticsEnzyme kinetics; Further Variations:Reaction partnersSolventsreaction time;
参考文献
Park, Heylin; Jung, Seunho
Carbohydrate Research, 2008 , vol. 343, # 2 p. 274 - 281
反应条件
sodium nitrite in acetic acid
参考文献
Ieda, Naoya; Nakagawa, Hidehiko; Peng, Tao; Yang, Dan; Suzuki, Takayoshi; Miyata, Naoki
Journal of the American Chemical Society, 2012 , vol. 134, # 5 p. 2563 - 2568