1: potassium carbonate / methanol; water / 4 h / 20 °C 2: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 3 h / 20 °C 3: acetic acid / water / 5.25 h / 0 °C 4: PPA / 1 h / 180 °C View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 10, # 12 p. 2389 - 2391
1: [{(η5-C5Me5)IrCl}2(μ-Cl)2] / toluene / 48 h / Inert atmosphere; Reflux 2: potassium carbonate / methanol; water / 4 h / 20 °C 3: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 3 h / 20 °C 4: acetic acid / water / 5.25 h / 0 °C 5: PPA / 1 h / 180 °C View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 10, # 12 p. 2389 - 2391
