4-苯并噁唑-2-苯甲腈合成路线 (共 22 条)
反应条件
cerium(IV) oxide in water
T=30°C; 0.333333 h;
参考文献
Shelkar, Radheshyam; Sarode, Sachin; Nagarkar, Jayashree
Tetrahedron Letters, 2013 , vol. 54, # 51 p. 6986 - 6990
反应条件
{PdCl2[(t-Bu)2PCl]2}; Cu[9,9-dimethyl-4,5-bis(diphenylphosphine)xanthene]I; caesium carbonate in toluene
T=100°C; Inert atmosphere;
参考文献
Huang, Jinkun; Chan, Johann; Chen, Ying; Borths, Christopher J.; Baucom, Kyle D.; Larsen, Robert D.; Faul, Margaret M.
Journal of the American Chemical Society, 2010 , vol. 132, # 11 p. 3674 - 3675
反应条件
Al3+ exchanged K10 clay in anhydrous xylene
T=140°C; 16 h; Green chemistry;
参考文献
Suresh, Dhanusu; Dhakshinamoorthy, Amarajothi; Pitchumani, Kasi
Tetrahedron Letters, 2013 , vol. 54, # 48 p. 6415 - 6419
反应条件
poly(ethylene glycol)-bound sulphonic acid in 1,4-dioxane; chloroform
T=60 - 65°C;
参考文献
Chikhale, Rupesh V.; Pant, Amit M.; Menghani, Sunil S.; Wadibhasme, Pankaj G.; Khedekar, Pramod B.
South African Journal of Chemistry, 2013 , vol. 66, p. 254 - 262
反应条件
1: With copper diacetate; palladium diacetate; trifluoroacetic acid in ethylene glycol dimethyl ether
T=120°C; 24 h; Inert atmosphereSealed tube;
2: With potassium carbonate in ethylene glycol dimethyl ether; water
T=20°C;
参考文献
Wang, Min; Li, Dengke; Zhou, Wei; Wang, Lei
Tetrahedron, 2012 , vol. 68, # 7 p. 1926 - 1930
反应条件
PdCl2(C3H3N2(CH3))(C3H2N2(C6H3(C3H7)2)2); lithium tert-butylate in toluene
T=130°C; 18 h; Inert atmosphere;
参考文献
Shen, Xiao-Bao; Zhang, Yun; Chen, Wen-Xin; Xiao, Zheng-Kang; Hu, Ting-Ting; Shao, Li-Xiong
Organic Letters, 2014 , vol. 16, # 7 p. 1984 - 1987
反应条件
copper(l) iodide; sodium carbonate; triphenylphosphine in N,N-dimethyl-formamide
T=160°C; 2 h;
参考文献
Yoshizumi, Tomoki; Tsurugi, Hayato; Satoh, Tetsuya; Miura, Masahiro
Tetrahedron Letters, 2008 , vol. 49, # 10 p. 1598 - 1600
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene; triphenylphosphine in conc HCl
参考文献
EASTMAN CHEMICAL COMPANY
Patent: EP479161 A1, 1992 ;
反应条件
dipotassium peroxodisulfate; 1,10-phenanthroline; palladium diacetate in dimethyl sulfoxide; toluene
T=120°C; 24 h; air; chemoselective reaction;
参考文献
Li, Chengliang; Li, Pinhua; Yang, Jin; Wang, Lei
Chemical Communications, 2012 , vol. 48, # 35 p. 4214 - 4216
反应条件
1: 76 percent / diethyl ether / 8 h / Ambient temperature
2: 52 percent / 6 h / 220 °C
View Scheme
参考文献
Wagner; Eppner
Pharmazie, 1980 , vol. 35, # 5-6 p. 285 - 288