2-(氯甲基)-4,4,5,5-四甲基-1,3,2-二噁硼烷合成路线 (共 14 条)
反应条件
in diethyl ether
at -78 to 23°C under Ar; 96-98 percent isomeric purity;
参考文献
Roush,W.R.; Adam,M.A.; Walts,A.E.
Journal of the American Chemical Society, 1986 , vol. 108, p. 3422
反应条件
in acetone
(Ar); refluxed for 48 h; volatiles distd., fractionally distd.; elem. anal.;
参考文献
Wuts, Peter G. M.; Thompson, Paul A.
Journal of Organometallic Chemistry, 1982 , vol. 234, # 2 p. 137 - 142
反应条件
in diethyl ether
at -78 to 23°C under Ar; various product ratios for various amts. of org. compd.;
参考文献
Roush,W.R.; Adam,M.A.; Walts,A.E.
Journal of the American Chemical Society, 1986 , vol. 108, p. 3422
反应条件
in tetrahydrofuran
at -78 to 23°C under Ar;
参考文献
Roush,W.R.; Adam,M.A.; Walts,A.E.
Journal of the American Chemical Society, 1986 , vol. 108, p. 3422