(E)-1-甲基-1,2二苯基乙烯合成路线 (共 175 条)
反应条件
iron-(III)-acetylacetonate; tributylphosphine; copper(I) bromide in diethyl ether T=30°C; 3 h; Inert atmosphere; optical yield given as percent destereoselective reaction;
参考文献
Chemical Communications, , # 14 p. 1885 - 1887
反应条件
1: benzyl bromide With bromine; zinc in tetrahydrofuran T=0 - 20°C; 1.5 h; Inert atmosphere; 2: acetophenone With AlCl3, aluminium chloride in tetrahydrofuran 12 h; Inert atmosphereReflux;
参考文献
Organic Letters, , vol. 13, # 8 p. 1996 - 1999
反应条件
1: benzyl halide With triphenylphosphine in ethyl acetate 5 h; Reflux; 2: With n-butyllithium T=0 - 20°C; 3: acetophenone Wittig reaction;
参考文献
Liu, Hua; Cao, Li; Sun, Jia; Fossey, John S.; Deng, Wei-Ping
Chemical Communications, 2012 , vol. 48, # 21 p. 2674 - 2676
反应条件
sodium acetate; bis(dibenzylideneacetone)-palladium(0) in dichloromethane 2 h; Ambient temperature;
参考文献
Kikukawa, K.; Nagira, K.; Wada, F.; Matsuda, T.
Tetrahedron, 1981 , vol. 37, p. 31 - 36
反应条件
in diethylene glycol dimethyl ether T=90 - 125°C;
参考文献
Tetrahedron Letters, , vol. 23, # 16 p. 1627 - 1630
反应条件
bis(acetylacetonate)nickel(II) in tetrahydrofuran T=20°C; 24 h;
参考文献
Bulletin de la Societe Chimique de France, , # 5 p. 762 - 771
反应条件
tetrakis(triphenylphosphine) palladium(0) in benzene T=80°C; 2 h; Further byproducts given;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 61, p. 3575 - 3580
反应条件
sodium acetate; iron(II) chloride in acetone T=-3 - 0°C; 1.5 h;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 27, p. 1988 - 1989
Zhurnal Organicheskoi Khimii, , vol. 27, # 10 p. 2244 - 2245
反应条件
[1,3-bis(diphenylphosphino) propane] dichloronickel(II) in diethyl ether; benzene 24 h; Ambient temperature;
参考文献
Tetrahedron, , vol. 51, # 16 p. 4691 - 4700
反应条件
NiCl2((PPh3)P)2 in tetrahydrofuran 48 h; Ambient temperature;
参考文献
Huang, Xian; Ma, Yun
Synthesis, 1997 , # 4 p. 417 - 419