(E)-1-甲基-1,2二苯基乙烯合成路线 (共 175 条)
参考文献
Journal of the American Chemical Society, , vol. 105, # 26 p. 7631 - 7637
反应条件
dimethyl sulfate; trifluoroacetic acid in tetrahydrofuran Heating a N2 satd. soln. of (CH3)2SO4 and boratirene on a steam bath.; Quenching with CF3CO2H, GC/MS.;
参考文献
Journal of the American Chemical Society, , vol. 113, # 6 p. 2155 - 2163
反应条件
1: With NiCl2((PPh3)P)2 in tetrahydrofuran 48 h; Inert atmosphereReflux; 2: With water; ammonium chloride in tetrahydrofuran T=20°C;
参考文献
Chen, Guiqin; Yu, Yan; Cai, Mingzhong
Synthetic Communications, 2009 , vol. 39, # 8 p. 1478 - 1487
反应条件
palladium diacetate; trifluoroacetic acid; 1,8-diamino-naphthalene in 1,4-dioxane; water T=120°C; 24 h; Inert atmosphereSealed tube; regioselective reaction;
参考文献
Liu, Saiwen; Bai, Yang; Cao, Xiangxiang; Xiao, Fuhong; Deng, Guo-Jun
Chemical Communications, 2013 , vol. 49, # 68 p. 7501 - 7503
反应条件
benzyl-N,N-dimethylamine; palladium diacetate in xylene T=130°C; 49 h;
参考文献
Journal of Organometallic Chemistry, , vol. 240, # 2 p. 209 - 216
反应条件
potassium carbonate; Pd-SAPO-31 in N,N-dimethyl-formamide T=120°C; Heck reaction; 12 h;
参考文献
Tetrahedron Letters, , vol. 44, # 18 p. 3649 - 3651
反应条件
2: azulene, benzophenone / 2-methyl-propan-2-ol / 30 °C / Irradiation; azulene effect; also in toluene View Scheme
参考文献
Journal of the American Chemical Society, , vol. 105, # 26 p. 7631 - 7637
反应条件
sulfuric acid in water T=20°C; Friedel Crafts acylation; 18 h;
参考文献
Journal of the Indian Chemical Society, , vol. 87, # 5 p. 595 - 600
反应条件
Pd(PPh3)4Cl2 in benzene T=80°C; 3 h;
参考文献
Journal of Organic Chemistry, , vol. 62, # 25 p. 8681 - 8686
反应条件
chromium dichloride; 2,2,2-trimethylacetic acid in toluene T=60°C; 18 h;
参考文献
Organic Letters, , vol. 9, # 8 p. 1569 - 1571