(E)-1-甲基-1,2二苯基乙烯合成路线 （共 175 条）
反应条件
[Rh((R,R)-Cy-SMS-Phos)(MeOH)2]BF4; hydrogen in methanol T=20°C; P=750.075 Torr; 20 h; optical yield given as percent ee;
参考文献
Organic Letters, , vol. 12, # 13 p. 3022 - 3025
反应条件
1: bromobenzene With per-6-guanidino-β-cyclodextrin; palladium diacetate in water; N,N-dimethyl-formamide 0.5 h; 2: trans-2-methylstyrene With potassium carbonate in water; N,N-dimethyl-formamide T=80°C; 11 h; Reagent/catalyst;
参考文献
Kanagaraj, Kuppusamy; Pitchumani, Kasi
Chemistry - A European Journal, 2013 , vol. 19, # 43 p. 14425 - 14431
反应条件
1: 1-bromo-1-phenyl-ethane With triphenylphosphine in ethyl acetate Wittig-Horner Reaction; 72 h; Reflux; 2: benzaldehyde With potassium tert-butylate in tetrahydrofuran Wittig-Horner Reaction; 5 h; Sealed tubeInert atmosphere; Overall yield = 59 percent; Overall yield = 0.94 g;
参考文献
Tetrahedron, , vol. 70, # 9 p. 1748 - 1762
反应条件
sulfuric acid; acetic acid Heating;
参考文献
Khalaf, Ali A.; Awad, Ibrahim M.; El-Emary; El-Aal, H.A.K. Abd
Journal of the Indian Chemical Society, 2010 , vol. 87, # 5 p. 595 - 600
反应条件
tetrakis(triphenylphosphine) palladium(0) in benzene T=80°C;
参考文献
Chemistry Letters, , p. 347 - 350
反应条件
water; acetic acid; bis-triphenylphosphine-palladium(II) chloride T=20°C; 6 h;
参考文献
Journal of Organic Chemistry, , vol. 73, # 2 p. 558 - 562
反应条件
sulfuric acid in water T=20°C; Friedel Crafts acylation; 2 h;
参考文献
Khalaf, Ali A.; Awad, Ibrahim M.; El-Emary; El-Aal, H.A.K. Abd
Journal of the Indian Chemical Society, 2010 , vol. 87, # 5 p. 595 - 600
反应条件
sodium acetate; bis(dibenzylideneacetone)-palladium(0) in dichloromethane 2 h; Ambient temperature;
参考文献
Kikukawa, K.; Nagira, K.; Wada, F.; Matsuda, T.
Tetrahedron, 1981 , vol. 37, p. 31 - 36
反应条件
lithium hydride; zinc(II) iodide; tetrakis(triphenylphosphine) palladium(0) 1.) THF, room temp., 3 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 60, # 2 p. 290 - 291
反应条件
acetic acid; tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane 5 h; Heating;
参考文献
Guo, Hao; Ma, Shengming
Synthesis, 2007 , # 17 p. 2731 - 2745
